Microstructure and composition analysis of nanostructured materials using HREM and FEG-TEM | |
Li, DX; Ping, DH; Huang, JY; Yu, YD; Ye, HQ | |
通讯作者 | Li, DX() |
2000-10-01 | |
发表期刊 | MICRON
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ISSN | 0968-4328 |
卷号 | 31期号:5页码:581-586 |
摘要 | The microstructure in nanostructured (NS) materials synthesized by different methods have been characterized by electron microscopy methods. NS-Pd was prepared by inert-gas condensation and in situ compacting method (IGCC), NS-alloys by amorphous crystallization method (ACM) and NS-Cu and Cu100-xFex alloy by mechanical alloying (MA) methods. The experimental results have revealed that different preparation techniques lead to different microstructures. The grain boundaries have ordered and disordered structures and high density of defects were frequently detected in NS-materials synthesized by IGCC and MA. For the NS-alloys produced by ACM, however, the structures of GBs are similar to those in coarse-grained materials and the grains have nearly perfect crystal structure. For immiscible systems, a supersaturated Fe-Cu solid solution can be obtained by MA, but it is difficult using IGCC. (C) 2000 Elsevier Science Ltd. All rights reserved. |
关键词 | nanostructured materials grain boundary defect structure solubility high-resolution electron microscope and field-emission-gun transmission electron microscope |
收录类别 | SCI |
语种 | 英语 |
WOS研究方向 | Microscopy |
WOS类目 | Microscopy |
WOS记录号 | WOS:000087050100017 |
出版者 | PERGAMON-ELSEVIER SCIENCE LTD |
引用统计 | |
文献类型 | 期刊论文 |
条目标识符 | http://ir.imr.ac.cn/handle/321006/110810 |
专题 | 中国科学院金属研究所 |
通讯作者 | Li, DX |
作者单位 | Chinese Acad Sci, Met Res Inst, Atom Imaging Solids Lab, Shenyang 110015, Peoples R China |
推荐引用方式 GB/T 7714 | Li, DX,Ping, DH,Huang, JY,et al. Microstructure and composition analysis of nanostructured materials using HREM and FEG-TEM[J]. MICRON,2000,31(5):581-586. |
APA | Li, DX,Ping, DH,Huang, JY,Yu, YD,&Ye, HQ.(2000).Microstructure and composition analysis of nanostructured materials using HREM and FEG-TEM.MICRON,31(5),581-586. |
MLA | Li, DX,et al."Microstructure and composition analysis of nanostructured materials using HREM and FEG-TEM".MICRON 31.5(2000):581-586. |
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