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XRD line broadening analysis with ball milled palladium
Lucks, I; Lamparter, P; Xu, J; Mittemeijer, EJ
Corresponding AuthorLucks, I()
2004
Source PublicationEUROPEAN POWDER DIFFRACTION EPDIC 8
ISSN0255-5476
Volume443-4Pages:119-122
AbstractPalladium powder was deformed by ball milling under an argon atmosphere in two types of mills for different milling times. Two methods for X-ray diffraction line profile analysis, the Williamson-Hall method and the Warren-Averbach method, yielded similar trends, but different quantitative results for crystallite sizes (column lengths) and microstrains. With both methods, from the anisotropic line broadening for planetary milled Pd smaller crystallite sizes and larger microstrains were obtained along the <100> direction than along <111>. Milling in a shaker mill causes microstrain higher by a factor of about two than milling in a planetary mill. The evolution of the crystallite size upon milling was discussed in terms of bimodal size distributions.
Keywordball milled Pd line broadening analysis X-ray diffraction
Indexed BySCI
Language英语
WOS Research AreaCrystallography ; Materials Science
WOS SubjectCrystallography ; Materials Science, Multidisciplinary
WOS IDWOS:000189421300024
PublisherTRANS TECH PUBLICATIONS LTD
Citation statistics
Cited Times:5[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.imr.ac.cn/handle/321006/120537
Collection中国科学院金属研究所
Corresponding AuthorLucks, I
Affiliation1.Max Planck Inst Met Res, DE-70569 Stuttgart, Germany
2.CAS, Shenyang Natl Lab Mat Sci, Inst Met Res, Shenyang 110016, Peoples R China
Recommended Citation
GB/T 7714
Lucks, I,Lamparter, P,Xu, J,et al. XRD line broadening analysis with ball milled palladium[J]. EUROPEAN POWDER DIFFRACTION EPDIC 8,2004,443-4:119-122.
APA Lucks, I,Lamparter, P,Xu, J,&Mittemeijer, EJ.(2004).XRD line broadening analysis with ball milled palladium.EUROPEAN POWDER DIFFRACTION EPDIC 8,443-4,119-122.
MLA Lucks, I,et al."XRD line broadening analysis with ball milled palladium".EUROPEAN POWDER DIFFRACTION EPDIC 8 443-4(2004):119-122.
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