XRD line broadening analysis with ball milled palladium

IMR OpenIR

	XRD line broadening analysis with ball milled palladium
	Lucks, I ; Lamparter, P ; Xu, J ; Mittemeijer, EJ
通讯作者	Lucks, I()
	2004
发表期刊	EUROPEAN POWDER DIFFRACTION EPDIC 8
ISSN	0255-5476
卷号	443-4 页码:119-122
摘要	Palladium powder was deformed by ball milling under an argon atmosphere in two types of mills for different milling times. Two methods for X-ray diffraction line profile analysis, the Williamson-Hall method and the Warren-Averbach method, yielded similar trends, but different quantitative results for crystallite sizes (column lengths) and microstrains. With both methods, from the anisotropic line broadening for planetary milled Pd smaller crystallite sizes and larger microstrains were obtained along the <100> direction than along <111>. Milling in a shaker mill causes microstrain higher by a factor of about two than milling in a planetary mill. The evolution of the crystallite size upon milling was discussed in terms of bimodal size distributions.
关键词	ball milled Pd line broadening analysis X-ray diffraction
收录类别	SCI
语种	英语
WOS研究方向	Crystallography ; Materials Science
WOS类目	Crystallography ; Materials Science, Multidisciplinary
WOS记录号	WOS:000189421300024
出版者	TRANS TECH PUBLICATIONS LTD
引用统计	被引频次：6[WOS] [WOS记录] [WOS相关记录]
文献类型	期刊论文
条目标识符	http://ir.imr.ac.cn/handle/321006/120537
专题	中国科学院金属研究所
通讯作者	Lucks, I
作者单位	1.Max Planck Inst Met Res, DE-70569 Stuttgart, Germany 2.CAS, Shenyang Natl Lab Mat Sci, Inst Met Res, Shenyang 110016, Peoples R China
推荐引用方式 GB/T 7714	Lucks, I,Lamparter, P,Xu, J,et al. XRD line broadening analysis with ball milled palladium[J]. EUROPEAN POWDER DIFFRACTION EPDIC 8,2004,443-4:119-122.
APA	Lucks, I,Lamparter, P,Xu, J,&Mittemeijer, EJ.(2004).XRD line broadening analysis with ball milled palladium.EUROPEAN POWDER DIFFRACTION EPDIC 8,443-4,119-122.
MLA	Lucks, I,et al."XRD line broadening analysis with ball milled palladium".EUROPEAN POWDER DIFFRACTION EPDIC 8 443-4(2004):119-122.