IMR OpenIR
Size and morphology-controlled synthesis of Ni3C nanoparticles in a TEG solution and their magnetic properties
Zhang, Yajing1; Zhu, Yuan1; Cao, Yan1; Li, Da2; Zhang, Zhidong2; Wang, Kangjun1; Ding, Fu1; Wang, Xiaolei3; Meng, Dan1; Fan, Lihui1; Wu, Jing1
Corresponding AuthorZhang, Yajing(yjzhang2009@163.com) ; Li, Da(dali@imr.ac.cn)
2016
Source PublicationRSC ADVANCES
ISSN2046-2069
Volume6Issue:85Pages:81989-81994
AbstractNickel carbide nanoparticles (Ni3C NPs) were synthesized by a polyol solution refluxing route at a temperature of 300 degrees C for 20 min using triphenylphosphine oxide (TPPO) as the surfactant. Size and morphologies of the Ni3C NPs were controlled by adjusting the concentration of Ni(NO3)(2) and TPPO. The products consisted of Ni and Ni3C could be kinetically controlled by a reaction temperature of 250-290 degrees C and time less than 20 min and the proportion of the Ni component was lower with longer reaction times and higher temperatures due to carbon atom insertion via a carbonaceous film that formed on the surface of the growing particles. The formation process of the Ni3C NPs was investigated by X-ray diffraction (XRD), scanning electron microscopy (SEM), high-resolution transmission electron microscopy (HRTEM), and X-ray photoelectron spectroscopy (XPS) characterization. The saturation magnetizations of products decreased with decreasing ratio of Ni : Ni3C, which inferred that Ni3C was non-magnetic and the magnetism arose from trace Ni in the products.
Funding OrganizationNational Nature Science Foundation of China ; SRF for ROCS, SEM ; Natural Science Foundation of Liaoning Province ; Science Research Foundation of Education Department of Liaoning Province ; LNET
DOI10.1039/c6ra11916f
Indexed BySCI
Language英语
Funding ProjectNational Nature Science Foundation of China[51301114] ; National Nature Science Foundation of China[51371175] ; National Nature Science Foundation of China[21201123] ; National Nature Science Foundation of China[21203125] ; National Nature Science Foundation of China[61403263] ; SRF for ROCS, SEM[[2010]1174] ; Natural Science Foundation of Liaoning Province[2015020649] ; Science Research Foundation of Education Department of Liaoning Province[L2015396] ; LNET[LJQ2013044]
WOS Research AreaChemistry
WOS SubjectChemistry, Multidisciplinary
WOS IDWOS:000382776000071
PublisherROYAL SOC CHEMISTRY
Citation statistics
Cited Times:16[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.imr.ac.cn/handle/321006/122595
Collection中国科学院金属研究所
Corresponding AuthorZhang, Yajing; Li, Da
Affiliation1.Shenyang Univ Chem Technol, Coll Chem Engn, Shenyang 110142, Peoples R China
2.Chinese Acad Sci, Shenyang Natl Lab Mat Sci, Inst Met Res, Shenyang 110016, Peoples R China
3.Shenyang Univ Technol, Sch Sci, Shenyang 110870, Peoples R China
Recommended Citation
GB/T 7714
Zhang, Yajing,Zhu, Yuan,Cao, Yan,et al. Size and morphology-controlled synthesis of Ni3C nanoparticles in a TEG solution and their magnetic properties[J]. RSC ADVANCES,2016,6(85):81989-81994.
APA Zhang, Yajing.,Zhu, Yuan.,Cao, Yan.,Li, Da.,Zhang, Zhidong.,...&Wu, Jing.(2016).Size and morphology-controlled synthesis of Ni3C nanoparticles in a TEG solution and their magnetic properties.RSC ADVANCES,6(85),81989-81994.
MLA Zhang, Yajing,et al."Size and morphology-controlled synthesis of Ni3C nanoparticles in a TEG solution and their magnetic properties".RSC ADVANCES 6.85(2016):81989-81994.
Files in This Item:
There are no files associated with this item.
Related Services
Recommend this item
Bookmark
Usage statistics
Export to Endnote
Google Scholar
Similar articles in Google Scholar
[Zhang, Yajing]'s Articles
[Zhu, Yuan]'s Articles
[Cao, Yan]'s Articles
Baidu academic
Similar articles in Baidu academic
[Zhang, Yajing]'s Articles
[Zhu, Yuan]'s Articles
[Cao, Yan]'s Articles
Bing Scholar
Similar articles in Bing Scholar
[Zhang, Yajing]'s Articles
[Zhu, Yuan]'s Articles
[Cao, Yan]'s Articles
Terms of Use
No data!
Social Bookmark/Share
All comments (0)
No comment.
 

Items in the repository are protected by copyright, with all rights reserved, unless otherwise indicated.