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A simple method for the synthesis of nanosized Ti3AlC2 powder in NaCl-KCl molten salt
Yang, Ling Xu1,2; Wang, Ying1,2; Zhang, Hai Liang1,2; Liu, Hui Jun1; Zeng, Chao Liu1
Corresponding AuthorLiu, Hui Jun(liuhj@imr.ac.cn)
2019
Source PublicationMATERIALS RESEARCH LETTERS
ISSN2166-3831
Volume7Issue:9Pages:361-367
AbstractHerein we report, a simple novel method to synthesize nanosized Ti3AlC2 powder from Ti, Al, and C powders in NaCl-KCl molten salt. It is more conducive to the formation of Ti3AlC2 at higher salt/precursor materials ratio and particle size of Ti3AlC2 powder dramatically decreases with increasing mass ratio of the salt to precursor materials. Fine-grained Ti3AlC2 powder is successfully synthesized at 950 degrees C for 5 h or at 1000 degrees C for 2 h with a salt/precursor materials ratio of 10:1. Ti3C2 MXene is also prepared by etching fine-grained Ti3AlC2 precursor in HF solution at 60 degrees C for 2 h. [GRAPHICS]
KeywordTernary carbide Ti3AlC2 nanosized powder molten salt microstructure
Funding OrganizationNational Natural Science Foundation of China
DOI10.1080/21663831.2019.1613695
Indexed BySCI
Language英语
Funding ProjectNational Natural Science Foundation of China[51501205]
WOS Research AreaMaterials Science
WOS SubjectMaterials Science, Multidisciplinary
WOS IDWOS:000471551600003
PublisherTAYLOR & FRANCIS INC
Citation statistics
Cited Times:8[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.imr.ac.cn/handle/321006/133975
Collection中国科学院金属研究所
Corresponding AuthorLiu, Hui Jun
Affiliation1.Chinese Acad Sci, Inst Met Res, Lab Corros & Protect, Shenyang 110016, Liaoning, Peoples R China
2.Univ Sci & Technol China, Sch Mat Sci & Engn, Hefei, Anhui, Peoples R China
Recommended Citation
GB/T 7714
Yang, Ling Xu,Wang, Ying,Zhang, Hai Liang,et al. A simple method for the synthesis of nanosized Ti3AlC2 powder in NaCl-KCl molten salt[J]. MATERIALS RESEARCH LETTERS,2019,7(9):361-367.
APA Yang, Ling Xu,Wang, Ying,Zhang, Hai Liang,Liu, Hui Jun,&Zeng, Chao Liu.(2019).A simple method for the synthesis of nanosized Ti3AlC2 powder in NaCl-KCl molten salt.MATERIALS RESEARCH LETTERS,7(9),361-367.
MLA Yang, Ling Xu,et al."A simple method for the synthesis of nanosized Ti3AlC2 powder in NaCl-KCl molten salt".MATERIALS RESEARCH LETTERS 7.9(2019):361-367.
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