A simple method for the synthesis of nanosized Ti3AlC2 powder in NaCl-KCl molten salt | |
Yang, Ling Xu1,2; Wang, Ying1,2; Zhang, Hai Liang1,2; Liu, Hui Jun1; Zeng, Chao Liu1 | |
Corresponding Author | Liu, Hui Jun(liuhj@imr.ac.cn) |
2019 | |
Source Publication | MATERIALS RESEARCH LETTERS
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ISSN | 2166-3831 |
Volume | 7Issue:9Pages:361-367 |
Abstract | Herein we report, a simple novel method to synthesize nanosized Ti3AlC2 powder from Ti, Al, and C powders in NaCl-KCl molten salt. It is more conducive to the formation of Ti3AlC2 at higher salt/precursor materials ratio and particle size of Ti3AlC2 powder dramatically decreases with increasing mass ratio of the salt to precursor materials. Fine-grained Ti3AlC2 powder is successfully synthesized at 950 degrees C for 5 h or at 1000 degrees C for 2 h with a salt/precursor materials ratio of 10:1. Ti3C2 MXene is also prepared by etching fine-grained Ti3AlC2 precursor in HF solution at 60 degrees C for 2 h. [GRAPHICS] |
Keyword | Ternary carbide Ti3AlC2 nanosized powder molten salt microstructure |
Funding Organization | National Natural Science Foundation of China |
DOI | 10.1080/21663831.2019.1613695 |
Indexed By | SCI |
Language | 英语 |
Funding Project | National Natural Science Foundation of China[51501205] |
WOS Research Area | Materials Science |
WOS Subject | Materials Science, Multidisciplinary |
WOS ID | WOS:000471551600003 |
Publisher | TAYLOR & FRANCIS INC |
Citation statistics | |
Document Type | 期刊论文 |
Identifier | http://ir.imr.ac.cn/handle/321006/133975 |
Collection | 中国科学院金属研究所 |
Corresponding Author | Liu, Hui Jun |
Affiliation | 1.Chinese Acad Sci, Inst Met Res, Lab Corros & Protect, Shenyang 110016, Liaoning, Peoples R China 2.Univ Sci & Technol China, Sch Mat Sci & Engn, Hefei, Anhui, Peoples R China |
Recommended Citation GB/T 7714 | Yang, Ling Xu,Wang, Ying,Zhang, Hai Liang,et al. A simple method for the synthesis of nanosized Ti3AlC2 powder in NaCl-KCl molten salt[J]. MATERIALS RESEARCH LETTERS,2019,7(9):361-367. |
APA | Yang, Ling Xu,Wang, Ying,Zhang, Hai Liang,Liu, Hui Jun,&Zeng, Chao Liu.(2019).A simple method for the synthesis of nanosized Ti3AlC2 powder in NaCl-KCl molten salt.MATERIALS RESEARCH LETTERS,7(9),361-367. |
MLA | Yang, Ling Xu,et al."A simple method for the synthesis of nanosized Ti3AlC2 powder in NaCl-KCl molten salt".MATERIALS RESEARCH LETTERS 7.9(2019):361-367. |
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