Optimization of mixed silanes agent solution and curing process for composite gamma-glycidoxypropyl trimethoxysilane (gamma-GPS)/bis-1.2-(triethoxysilyl)ethane (BTSE) silane film on Q235 steel surfaceOptimierung von vermengten Silanlosungen und Aushartung fur gamma-glycidoxypropyl trimethoxysilan (gamma-GPS)/bis-1,2-(triethoxysilyl)athan (BTSE)-Komposit-Silanschicht auf einer Stahloberflache (Q 235)

doi:10.1002/mawe.201900150

IMR OpenIR

	Optimization of mixed silanes agent solution and curing process for composite gamma-glycidoxypropyl trimethoxysilane (gamma-GPS)/bis-1.2-(triethoxysilyl)ethane (BTSE) silane film on Q235 steel surfaceOptimierung von vermengten Silanlosungen und Aushartung fur gamma-glycidoxypropyl trimethoxysilan (gamma-GPS)/bis-1,2-(triethoxysilyl)athan (BTSE)-Komposit-Silanschicht auf einer Stahloberflache (Q 235)
	Sun, Z. D.1,2,3; Yang, Y. N.1; Li, Q. K.3; Liu, J. G.3; Xu, Q.1,4; Yan, C. W.3
Corresponding Author	Sun, Z. D.(sunzd@sie.edu.cn)
	2020-04-01
Source Publication	MATERIALWISSENSCHAFT UND WERKSTOFFTECHNIK
ISSN	0933-5137
Volume	51 Issue:4 Pages:480-487
Abstract	In this investigation, the mixed gamma-GPS/BTSE silane solution for preparing well adhered composite gamma-GPS/BTSE silane film on Q235 carbon steel surface has been successfully optimized by orthogonal test, and the curing process parameters of temperature and time have also been optimized. The results indicate that the optimized hydrolysis parameters for mixed silanes agent solution are as follows: V-ethanol/V-water 3 : 1, V gamma-GPS/V-BTSE 2 : 3, V-silanes 6 vol.%, pH 4.0 and hydrolysis time 72 h. In addition, the optimized curing condition for composite gamma-GPS/BTSE silane film is 120 degrees C and 30 min. After immersion in the optimized mixed gamma-GPS/BTSE silanes agent solution and curing under the optimized condition, the prepared composite gamma-GPS/BTSE silane film on Q235 steel surface can have an adhesion strength of 24.52 MPa to underlying steel substrate.
Keyword	Epoxy resin silane treatment orthogonal test adhesion Q235 steel
DOI	10.1002/mawe.201900150
Indexed By	SCI
Language	英语
WOS Research Area	Materials Science
WOS Subject	Materials Science, Multidisciplinary
WOS ID	WOS:000525608800008
Publisher	WILEY-V C H VERLAG GMBH
Citation statistics	Cited Times:1[WOS] [WOS Record] [Related Records in WOS]
Document Type	期刊论文
Identifier	http://ir.imr.ac.cn/handle/321006/138356
Collection	中国科学院金属研究所
Corresponding Author	Sun, Z. D.
Affiliation	1.Northeastern Univ, Sch Met, Shenyang 110819, Peoples R China 2.Shenyang Inst Engn, Shenyang 110136, Peoples R China 3.Chinese Acad Sci, Inst Met Res, Lab Corros & Protect Met, Shenyang 110016, Peoples R China 4.Shanghai Univ, Sch Mat Sci & Engn, State Key Lab Adv Special Steel, Shanghai 200072, Peoples R China
Recommended Citation GB/T 7714	Sun, Z. D.,Yang, Y. N.,Li, Q. K.,et al. Optimization of mixed silanes agent solution and curing process for composite gamma-glycidoxypropyl trimethoxysilane (gamma-GPS)/bis-1.2-(triethoxysilyl)ethane (BTSE) silane film on Q235 steel surfaceOptimierung von vermengten Silanlosungen und Aushartung fur gamma-glycidoxypropyl trimethoxysilan (gamma-GPS)/bis-1,2-(triethoxysilyl)athan (BTSE)-Komposit-Silanschicht auf einer Stahloberflache (Q 235)[J]. MATERIALWISSENSCHAFT UND WERKSTOFFTECHNIK,2020,51(4):480-487.
APA	Sun, Z. D.,Yang, Y. N.,Li, Q. K.,Liu, J. G.,Xu, Q.,&Yan, C. W..(2020).Optimization of mixed silanes agent solution and curing process for composite gamma-glycidoxypropyl trimethoxysilane (gamma-GPS)/bis-1.2-(triethoxysilyl)ethane (BTSE) silane film on Q235 steel surfaceOptimierung von vermengten Silanlosungen und Aushartung fur gamma-glycidoxypropyl trimethoxysilan (gamma-GPS)/bis-1,2-(triethoxysilyl)athan (BTSE)-Komposit-Silanschicht auf einer Stahloberflache (Q 235).MATERIALWISSENSCHAFT UND WERKSTOFFTECHNIK,51(4),480-487.
MLA	Sun, Z. D.,et al."Optimization of mixed silanes agent solution and curing process for composite gamma-glycidoxypropyl trimethoxysilane (gamma-GPS)/bis-1.2-(triethoxysilyl)ethane (BTSE) silane film on Q235 steel surfaceOptimierung von vermengten Silanlosungen und Aushartung fur gamma-glycidoxypropyl trimethoxysilan (gamma-GPS)/bis-1,2-(triethoxysilyl)athan (BTSE)-Komposit-Silanschicht auf einer Stahloberflache (Q 235)".MATERIALWISSENSCHAFT UND WERKSTOFFTECHNIK 51.4(2020):480-487.

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