Optimization of mixed silanes agent solution and curing process for composite gamma-glycidoxypropyl trimethoxysilane (gamma-GPS)/bis-1.2-(triethoxysilyl)ethane (BTSE) silane film on Q235 steel surfaceOptimierung von vermengten Silanlosungen und Aushartung fur gamma-glycidoxypropyl trimethoxysilan (gamma-GPS)/bis-1,2-(triethoxysilyl)athan (BTSE)-Komposit-Silanschicht auf einer Stahloberflache (Q 235)

doi:10.1002/mawe.201900150

IMR OpenIR

	Optimization of mixed silanes agent solution and curing process for composite gamma-glycidoxypropyl trimethoxysilane (gamma-GPS)/bis-1.2-(triethoxysilyl)ethane (BTSE) silane film on Q235 steel surfaceOptimierung von vermengten Silanlosungen und Aushartung fur gamma-glycidoxypropyl trimethoxysilan (gamma-GPS)/bis-1,2-(triethoxysilyl)athan (BTSE)-Komposit-Silanschicht auf einer Stahloberflache (Q 235)
	Sun, Z. D.1,2,3; Yang, Y. N.1; Li, Q. K.3; Liu, J. G.3; Xu, Q.1,4; Yan, C. W.3
通讯作者	Sun, Z. D.(sunzd@sie.edu.cn)
	2020-04-01
发表期刊	MATERIALWISSENSCHAFT UND WERKSTOFFTECHNIK
ISSN	0933-5137
卷号	51 期号:4 页码:480-487
摘要	In this investigation, the mixed gamma-GPS/BTSE silane solution for preparing well adhered composite gamma-GPS/BTSE silane film on Q235 carbon steel surface has been successfully optimized by orthogonal test, and the curing process parameters of temperature and time have also been optimized. The results indicate that the optimized hydrolysis parameters for mixed silanes agent solution are as follows: V-ethanol/V-water 3 : 1, V gamma-GPS/V-BTSE 2 : 3, V-silanes 6 vol.%, pH 4.0 and hydrolysis time 72 h. In addition, the optimized curing condition for composite gamma-GPS/BTSE silane film is 120 degrees C and 30 min. After immersion in the optimized mixed gamma-GPS/BTSE silanes agent solution and curing under the optimized condition, the prepared composite gamma-GPS/BTSE silane film on Q235 steel surface can have an adhesion strength of 24.52 MPa to underlying steel substrate.
关键词	Epoxy resin silane treatment orthogonal test adhesion Q235 steel
DOI	10.1002/mawe.201900150
收录类别	SCI
语种	英语
WOS研究方向	Materials Science
WOS类目	Materials Science, Multidisciplinary
WOS记录号	WOS:000525608800008
出版者	WILEY-V C H VERLAG GMBH
引用统计	被引频次：2[WOS] [WOS记录] [WOS相关记录]
文献类型	期刊论文
条目标识符	http://ir.imr.ac.cn/handle/321006/138356
专题	中国科学院金属研究所
通讯作者	Sun, Z. D.
作者单位	1.Northeastern Univ, Sch Met, Shenyang 110819, Peoples R China 2.Shenyang Inst Engn, Shenyang 110136, Peoples R China 3.Chinese Acad Sci, Inst Met Res, Lab Corros & Protect Met, Shenyang 110016, Peoples R China 4.Shanghai Univ, Sch Mat Sci & Engn, State Key Lab Adv Special Steel, Shanghai 200072, Peoples R China
推荐引用方式 GB/T 7714	Sun, Z. D.,Yang, Y. N.,Li, Q. K.,et al. Optimization of mixed silanes agent solution and curing process for composite gamma-glycidoxypropyl trimethoxysilane (gamma-GPS)/bis-1.2-(triethoxysilyl)ethane (BTSE) silane film on Q235 steel surfaceOptimierung von vermengten Silanlosungen und Aushartung fur gamma-glycidoxypropyl trimethoxysilan (gamma-GPS)/bis-1,2-(triethoxysilyl)athan (BTSE)-Komposit-Silanschicht auf einer Stahloberflache (Q 235)[J]. MATERIALWISSENSCHAFT UND WERKSTOFFTECHNIK,2020,51(4):480-487.
APA	Sun, Z. D.,Yang, Y. N.,Li, Q. K.,Liu, J. G.,Xu, Q.,&Yan, C. W..(2020).Optimization of mixed silanes agent solution and curing process for composite gamma-glycidoxypropyl trimethoxysilane (gamma-GPS)/bis-1.2-(triethoxysilyl)ethane (BTSE) silane film on Q235 steel surfaceOptimierung von vermengten Silanlosungen und Aushartung fur gamma-glycidoxypropyl trimethoxysilan (gamma-GPS)/bis-1,2-(triethoxysilyl)athan (BTSE)-Komposit-Silanschicht auf einer Stahloberflache (Q 235).MATERIALWISSENSCHAFT UND WERKSTOFFTECHNIK,51(4),480-487.
MLA	Sun, Z. D.,et al."Optimization of mixed silanes agent solution and curing process for composite gamma-glycidoxypropyl trimethoxysilane (gamma-GPS)/bis-1.2-(triethoxysilyl)ethane (BTSE) silane film on Q235 steel surfaceOptimierung von vermengten Silanlosungen und Aushartung fur gamma-glycidoxypropyl trimethoxysilan (gamma-GPS)/bis-1,2-(triethoxysilyl)athan (BTSE)-Komposit-Silanschicht auf einer Stahloberflache (Q 235)".MATERIALWISSENSCHAFT UND WERKSTOFFTECHNIK 51.4(2020):480-487.