The Influences of Stirring on the Recrystallization of Ammonium Perrhenate

doi:10.3390/app10020656

IMR OpenIR

	The Influences of Stirring on the Recrystallization of Ammonium Perrhenate
	Tang, Junjie 1,2,3; Feng, Li 4; Zhang, Chunwei 3,5; Sun, Yuan 3; Wang, Long 3; Zhou, Yizhou 3; Fang, Dawei 5; Liu, Yan 2
通讯作者	Tang, Junjie(tangjunjieyh@lnist.edu.cn) ; Sun, Yuan(yuansun@imr.ac.cn) ; Zhou, Yizhou(yzzhou@imr.ac.cn)
	2020
发表期刊	APPLIED SCIENCES-BASEL
卷号	10 期号:2 页码:11
摘要	Ammonium perrhenate is widely used in alloy manufacturing, powder processing, the catalytic industry, and other fields. Recrystallization can improve the specific surface area of ammonium perrhenate, reduce its particle size, and improve its particle size distribution uniformity. Therefore, recrystallized ammonium perrhenate can obtain better application benefits in the above fields. Stirring is an important factor that affects the recrystallization of ammonium perrhenate, and this paper systematically analyzes the influence of the stirring paddle types and stirring intensities on ammonium perrhenate during the homogeneous recrystallization process, ultimately revealing the relationship between the growth rate of ammonium perrhenate and the stirring process. Particle image velocimetry physical simulation results showed that the flow field in the reactor was more evenly distributed when using the disc turbine impeller, and a relatively uniform velocity liquid flow area was formed in the whole reactor, while the low-velocity liquid flow area was smaller. Therefore, this information, combined with SEM test results, suggests that under the same recrystallization time and stirring intensity, the stirring effect of a disc turbine impeller is more suitable than a propelling propeller and an Intermig impeller for the recrystallization process of ammonium perrhenate. Moreover, the XRD patterns and SEM analysis showed that if the agglomeration in the systems was too strong or too weak, the growths of the (101) crystal plane and (112) crystal plane were restrained, which caused an attenuation in the growth rates along the crystallographic directions that were orthogonal to the crystal faces. Finally, the reduction experiments show that the recrystallization of ammonium perrhenate could improve the phase parameters of rhenium powders.
关键词	ammonium perrhenate recrystallization stirring paddle type agglomeration
资助者	key laboratory of ecological metallurgy of polymetallic symbiosis in ministry of education, Northeastern University ; Liaoning provincial department of science and technology doctoral research initiation fund
DOI	10.3390/app10020656
收录类别	SCI
语种	英语
资助项目	key laboratory of ecological metallurgy of polymetallic symbiosis in ministry of education, Northeastern University[NEMM2019003] ; Liaoning provincial department of science and technology doctoral research initiation fund[2019-BS-130]
WOS研究方向	Chemistry ; Engineering ; Materials Science ; Physics
WOS类目	Chemistry, Multidisciplinary ; Engineering, Multidisciplinary ; Materials Science, Multidisciplinary ; Physics, Applied
WOS记录号	WOS:000522540400232
出版者	MDPI
引用统计	被引频次：5[WOS] [WOS记录] [WOS相关记录]
文献类型	期刊论文
条目标识符	http://ir.imr.ac.cn/handle/321006/138436
专题	中国科学院金属研究所
通讯作者	Tang, Junjie; Sun, Yuan; Zhou, Yizhou
作者单位	1.Liaoning Inst Sci & Technol, Sch Biomed & Chem Engn, Benxi 117004, Peoples R China 2.Northeastern Univ, Minist Educ, Key Lab Ecol Utilizat Multimetall Mineral, Shenyang 110819, Peoples R China 3.Chinese Acad Sci, Inst Met Res, Shenyang 110016, Peoples R China 4.Shenyang Polytech Coll, Elect Engn, Shenyang 110045, Peoples R China 5.Liaoning Univ, Coll Chem, Shenyang 110036, Peoples R China
推荐引用方式 GB/T 7714	Tang, Junjie,Feng, Li,Zhang, Chunwei,et al. The Influences of Stirring on the Recrystallization of Ammonium Perrhenate[J]. APPLIED SCIENCES-BASEL,2020,10(2):11.
APA	Tang, Junjie.,Feng, Li.,Zhang, Chunwei.,Sun, Yuan.,Wang, Long.,...&Liu, Yan.(2020).The Influences of Stirring on the Recrystallization of Ammonium Perrhenate.APPLIED SCIENCES-BASEL,10(2),11.
MLA	Tang, Junjie,et al."The Influences of Stirring on the Recrystallization of Ammonium Perrhenate".APPLIED SCIENCES-BASEL 10.2(2020):11.