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Preparation of transparent Y2O3 ceramic by slip casting and vacuum sintering
其他题名Preparation of transparent Y2O3 ceramic by slip casting and vacuum sintering
Huo Di1; Zheng Yanchun2; Sun Xudong1; Li Xiaodong1; Liu Shaohong1
2012
发表期刊JOURNAL OF RARE EARTHS
ISSN1002-0721
卷号30期号:1页码:57-62
摘要In the present work transparent Y2O3 ceramics were made by slip casting and vacuum sintering of nanopowders with sodium polyacrylic acid (PAA-Na) as dispersant. The rheological properties of Y2O3 nanopowder slurry were investigated using different amounts of dispersant and solid contents. The microstructures and transmittance of the sintered ceramics were also studied by means of scanning electron microscopy (SEM) and ultra-violet visible spectrometry. The results showed that rheological behaviors of the Y2O3 nanopowder slurry were effectively promoted by sodium polyacrylic acid. Highly dispersive and stable slurries were obtained as the dispersant was added over 1.0 dwb% under the fixed conditions of pH 11 and 45 wt.% solid content. All the slip cast green bodies were sintered into highly dense ceramics after sintering at 1700 degrees C for 5 h in vacuum, wherein the sample added with 1.1% sodium polyacrylic acid exhibited the highest relative density of 99.36% and transmission of 30% at 800 nm wavelength.
其他摘要In the present work transparent Y_2O_3 ceramics were made by slip casting and vacuum sintering of nanopowders with sodium poly-acrylic acid(PAA-Na) as dispersant.The rheological properties of Y_2O_3 nanopowder slurry were investigated using different amounts of dis-persant and solid contents.The microstructures and transmittance of the sintered ceramics were also studied by means of scanning electron microscopy(SEM) and ultra-violet visible spectrometry.The results showed that rheological behaviors of the Y_2O_3 nanopowder slurry were effectively promoted by sodium polyacrylic acid.Highly dispersive and stable slurries were obtained as the dispersant was added over 1.0 dwb% under the fixed conditions of pH 11 and 45 wt.% solid content.All the slip cast green bodies were sintered into highly dense ceramics after sintering at 1700 oC for 5 h in vacuum,wherein the sample added with 1.1% sodium polyacrylic acid exhibited the highest relative den-sity of 99.36% and transmission of 30% at 800 nm wavelength.
关键词SUSPENSIONS STABILITY RELIABILITY ALUMINA YTTRIA nanopowders yttria slip casting transparent ceramic sodium polyacrylic acid rare earths
收录类别CSCD
语种英语
资助项目[Liaoning Provincial Natural Science Foundation] ; [National Natural Science Foundation of China]
CSCD记录号CSCD:4443997
引用统计
文献类型期刊论文
条目标识符http://ir.imr.ac.cn/handle/321006/143801
专题中国科学院金属研究所
作者单位1.上海市地震局
2.中国科学院金属研究所
推荐引用方式
GB/T 7714
Huo Di,Zheng Yanchun,Sun Xudong,et al. Preparation of transparent Y2O3 ceramic by slip casting and vacuum sintering[J]. JOURNAL OF RARE EARTHS,2012,30(1):57-62.
APA Huo Di,Zheng Yanchun,Sun Xudong,Li Xiaodong,&Liu Shaohong.(2012).Preparation of transparent Y2O3 ceramic by slip casting and vacuum sintering.JOURNAL OF RARE EARTHS,30(1),57-62.
MLA Huo Di,et al."Preparation of transparent Y2O3 ceramic by slip casting and vacuum sintering".JOURNAL OF RARE EARTHS 30.1(2012):57-62.
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