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Synthesis, characterization and electromagnetic studies on nanocrystalline nickel zinc ferrite by polyacrylamide gel
Alternative TitleSynthesis, Characterization and Electromagnetic Studies on Nanocrystalline Nickel Zinc Ferrite by Polyacrylamide Gel
Ma Ruiting; Wang Yi; Tian Yanwen; Zhang Chunli; Li Xikun
2008
Source PublicationJOURNAL OF MATERIALS SCIENCE & TECHNOLOGY
ISSN1005-0302
Volume24Issue:3Pages:419-422
AbstractNanocrystalline nickel zinc ferrite powders (NixZn1-xFe2O4, A for x=0, B for x=0.2, C for x=0.5, D for x=0.8 and E for x= 1) were synthesized by polyacrylamide gel method. X-ray diffraction (XRD), transmission electron microscopy (TEM) and wave-guide were used to characterize the composition. The XRD results show that the dried gel powders are amorphous, and the characteristic peaks of the spinel Ni0.5Zn0.5Fe2O4 appear after the gel is calcined at 400 degrees C for I h. When the calcining temperatures are 600 and 800 degrees C, the average grain sizes are identified by TEM to be 10 and 30 nm, respectively. The NixZn1-xFe2O4 powders have both dielectric loss and magnetic loss in the frequency range of 8.2-11.0GHz. With the increase of Ni2+ ions content, the dielectric parameters (epsilon') and permeability (u') of the NixZn1-xFe2O4 powders decrease while the dielectric loss (epsilon ''), magnetic loss (u '') and the reflection loss increase.
Other AbstractNanocrystalline nickel zinc ferrite powders (NixZn1-xFe2O4, A for x=0, B for x=0.2, C for x=0.5, D for x= 0.8 and E for x= 1) were synthesized by polyacrylamide gel method. X-ray diffraction (XRD), transmission electron microscopy (TEM) and wave-guide were used to characterize the composition. The XRD results show that the dried gel powders are amorphous, and the characteristic peaks of the spinel Ni0.5Zn0.5Fe2O4 appear after the gel is calcined at 400℃ for 1 h. When the calcining temperatures are 600 and 800℃, the average grain sizes are identified by TEM to be 10 and 30 nm, respectively. The NixZn1-xFe2O4 powders have both.dielectric loss and magnetic loss in the frequency range of 8.2-11.0GHz. With the increase of Ni2+ ions content, the dielectric parameters (ε′) and permeability (u′) of the NixZn1-xFe2O4 powders decrease while the dielectric loss (ε″), magnetic loss (u″) and the reflection loss increase.
KeywordNI-ZN-FERRITE MAGNETIC-PROPERTIES COMBUSTION SYNTHESIS NANOCOMPOSITES PARTICLES POWDERS nanocrystalline ferrite electromagnetic properties polyacrylamide gel
Indexed ByCSCD
Language英语
CSCD IDCSCD:3316356
Citation statistics
Document Type期刊论文
Identifierhttp://ir.imr.ac.cn/handle/321006/144628
Collection中国科学院金属研究所
Affiliation中国科学院金属研究所
Recommended Citation
GB/T 7714
Ma Ruiting,Wang Yi,Tian Yanwen,et al. Synthesis, characterization and electromagnetic studies on nanocrystalline nickel zinc ferrite by polyacrylamide gel[J]. JOURNAL OF MATERIALS SCIENCE & TECHNOLOGY,2008,24(3):419-422.
APA Ma Ruiting,Wang Yi,Tian Yanwen,Zhang Chunli,&Li Xikun.(2008).Synthesis, characterization and electromagnetic studies on nanocrystalline nickel zinc ferrite by polyacrylamide gel.JOURNAL OF MATERIALS SCIENCE & TECHNOLOGY,24(3),419-422.
MLA Ma Ruiting,et al."Synthesis, characterization and electromagnetic studies on nanocrystalline nickel zinc ferrite by polyacrylamide gel".JOURNAL OF MATERIALS SCIENCE & TECHNOLOGY 24.3(2008):419-422.
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