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Synthesis, characterization and electromagnetic studies on nanocrystalline nickel zinc ferrite by polyacrylamide gel
其他题名Synthesis, Characterization and Electromagnetic Studies on Nanocrystalline Nickel Zinc Ferrite by Polyacrylamide Gel
Ma Ruiting; Wang Yi; Tian Yanwen; Zhang Chunli; Li Xikun
2008
发表期刊JOURNAL OF MATERIALS SCIENCE & TECHNOLOGY
ISSN1005-0302
卷号24期号:3页码:419-422
摘要Nanocrystalline nickel zinc ferrite powders (NixZn1-xFe2O4, A for x=0, B for x=0.2, C for x=0.5, D for x=0.8 and E for x= 1) were synthesized by polyacrylamide gel method. X-ray diffraction (XRD), transmission electron microscopy (TEM) and wave-guide were used to characterize the composition. The XRD results show that the dried gel powders are amorphous, and the characteristic peaks of the spinel Ni0.5Zn0.5Fe2O4 appear after the gel is calcined at 400 degrees C for I h. When the calcining temperatures are 600 and 800 degrees C, the average grain sizes are identified by TEM to be 10 and 30 nm, respectively. The NixZn1-xFe2O4 powders have both dielectric loss and magnetic loss in the frequency range of 8.2-11.0GHz. With the increase of Ni2+ ions content, the dielectric parameters (epsilon') and permeability (u') of the NixZn1-xFe2O4 powders decrease while the dielectric loss (epsilon ''), magnetic loss (u '') and the reflection loss increase.
其他摘要Nanocrystalline nickel zinc ferrite powders (NixZn1-xFe2O4, A for x=0, B for x=0.2, C for x=0.5, D for x= 0.8 and E for x= 1) were synthesized by polyacrylamide gel method. X-ray diffraction (XRD), transmission electron microscopy (TEM) and wave-guide were used to characterize the composition. The XRD results show that the dried gel powders are amorphous, and the characteristic peaks of the spinel Ni0.5Zn0.5Fe2O4 appear after the gel is calcined at 400℃ for 1 h. When the calcining temperatures are 600 and 800℃, the average grain sizes are identified by TEM to be 10 and 30 nm, respectively. The NixZn1-xFe2O4 powders have both.dielectric loss and magnetic loss in the frequency range of 8.2-11.0GHz. With the increase of Ni2+ ions content, the dielectric parameters (ε′) and permeability (u′) of the NixZn1-xFe2O4 powders decrease while the dielectric loss (ε″), magnetic loss (u″) and the reflection loss increase.
关键词NI-ZN-FERRITE MAGNETIC-PROPERTIES COMBUSTION SYNTHESIS NANOCOMPOSITES PARTICLES POWDERS nanocrystalline ferrite electromagnetic properties polyacrylamide gel
收录类别CSCD
语种英语
CSCD记录号CSCD:3316356
引用统计
文献类型期刊论文
条目标识符http://ir.imr.ac.cn/handle/321006/144628
专题中国科学院金属研究所
作者单位中国科学院金属研究所
推荐引用方式
GB/T 7714
Ma Ruiting,Wang Yi,Tian Yanwen,et al. Synthesis, characterization and electromagnetic studies on nanocrystalline nickel zinc ferrite by polyacrylamide gel[J]. JOURNAL OF MATERIALS SCIENCE & TECHNOLOGY,2008,24(3):419-422.
APA Ma Ruiting,Wang Yi,Tian Yanwen,Zhang Chunli,&Li Xikun.(2008).Synthesis, characterization and electromagnetic studies on nanocrystalline nickel zinc ferrite by polyacrylamide gel.JOURNAL OF MATERIALS SCIENCE & TECHNOLOGY,24(3),419-422.
MLA Ma Ruiting,et al."Synthesis, characterization and electromagnetic studies on nanocrystalline nickel zinc ferrite by polyacrylamide gel".JOURNAL OF MATERIALS SCIENCE & TECHNOLOGY 24.3(2008):419-422.
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