IMR OpenIR
PREPARATION AND CHARACTERIZATION OF CaB6 BY MOLTEN SALT ELECTROLYSIS
Alternative TitlePREPARATION AND CHARACTERIZATION OF CaB_6 BY MOLTEN SALT ELECTROLYSIS
Wang Xu; Zhai Yuchun; Xie Hongwei
2008
Source PublicationACTA METALLURGICA SINICA
ISSN0412-1961
Volume44Issue:10Pages:1243-1246
AbstractCaB6 powder was synthesized by molten salt electrolysis method, and the effects of synthesis temperature, electrolysis voltage and time on the phase composition, particle size and shape of cathode products were analyzed by XRD and SEM. The experimental results show that the best synthesis conditions of CaB6 powder in CaCl2 Molten salt system are: environment of argon, voltage of 3.0 V, temperature of 900 degrees C for 30 h, under which the range of CaB6 crystal size is 2-8 mu m and the morphology of particles is cuboid massive shape. Using cyclic voltammetry in cathode process, it is proved that the electrolysis process is controlled by the diffusion rate of borate to the cathode.
KeywordELECTROCHEMICAL REDUCTION TITANIUM-DIOXIDE CALCIUM-CHLORIDE EXTRACTION ALLOYS POWDER molten salt electrolysis molten salt system CaB6 diffusion rate cyclic voltammetry
Indexed ByCSCD
Language英语
CSCD IDCSCD:3420311
Citation statistics
Document Type期刊论文
Identifierhttp://ir.imr.ac.cn/handle/321006/152813
Collection中国科学院金属研究所
Affiliation中国科学院金属研究所
Recommended Citation
GB/T 7714
Wang Xu,Zhai Yuchun,Xie Hongwei. PREPARATION AND CHARACTERIZATION OF CaB6 BY MOLTEN SALT ELECTROLYSIS[J]. ACTA METALLURGICA SINICA,2008,44(10):1243-1246.
APA Wang Xu,Zhai Yuchun,&Xie Hongwei.(2008).PREPARATION AND CHARACTERIZATION OF CaB6 BY MOLTEN SALT ELECTROLYSIS.ACTA METALLURGICA SINICA,44(10),1243-1246.
MLA Wang Xu,et al."PREPARATION AND CHARACTERIZATION OF CaB6 BY MOLTEN SALT ELECTROLYSIS".ACTA METALLURGICA SINICA 44.10(2008):1243-1246.
Files in This Item:
There are no files associated with this item.
Related Services
Recommend this item
Bookmark
Usage statistics
Export to Endnote
Google Scholar
Similar articles in Google Scholar
[Wang Xu]'s Articles
[Zhai Yuchun]'s Articles
[Xie Hongwei]'s Articles
Baidu academic
Similar articles in Baidu academic
[Wang Xu]'s Articles
[Zhai Yuchun]'s Articles
[Xie Hongwei]'s Articles
Bing Scholar
Similar articles in Bing Scholar
[Wang Xu]'s Articles
[Zhai Yuchun]'s Articles
[Xie Hongwei]'s Articles
Terms of Use
No data!
Social Bookmark/Share
All comments (0)
No comment.
 

Items in the repository are protected by copyright, with all rights reserved, unless otherwise indicated.