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A novel ultra-low current and temperature controlled electrochemical method for exposing various kinds of secondary phase precipitates: Application to the sample preparation of zirconium alloys and some other common alloys
Han, Fuzhou1,2; Li, Geping2; Yuan, Fusen1,2; Ali, Muhammad1,2; Zhang, Yingdong1,2; Guo, Wenbin1,2; Ren, Jie1,2; Liu, Chengze1,2; Gu, Hengfei2,3
通讯作者Li, Geping(gpli@imr.ac.cn)
2021-06-01
发表期刊MATERIALS CHEMISTRY AND PHYSICS
ISSN0254-0584
卷号265页码:9
摘要Secondary phase particles (SPPs) have attracted extensive attention because of their effects on the properties and performance of alloy materials. In the present study, a novel ultra-low current and temperature controlled electrochemical (ULCT) method, which can expose contained SPPs on the alloy surface, has been proposed for the first time. We demonstrated that the exciting new approach is feasible for the high-quality bulk sample preparation of various common alloys including Zircaloy-4 (Zr-4 alloy), GH99 super alloy and 2A12 aluminium alloy. Results show that this ULCT method is a real universal and promising method for the specific sample preparation, which will make SEM-based techniques become invaluable for routine characterization of SPPs in various kinds of alloys.
关键词Novel electrochemical method Specific sample preparation Secondary precipitate phases (SPPs) Common metallic alloys
DOI10.1016/j.matchemphys.2021.124506
收录类别SCI
语种英语
WOS研究方向Materials Science
WOS类目Materials Science, Multidisciplinary
WOS记录号WOS:000643732700003
出版者ELSEVIER SCIENCE SA
引用统计
文献类型期刊论文
条目标识符http://ir.imr.ac.cn/handle/321006/162100
专题中国科学院金属研究所
通讯作者Li, Geping
作者单位1.Univ Sci & Technol China, Sch Mat Sci & Engn, 72 Wenhua Rd, Shenyang 110016, Peoples R China
2.Chinese Acad Sci, Shi Changxu Innovat Ctr Advanved Mat, Inst Met Res, 72 Wenhua Rd, Shenyang 110016, Peoples R China
3.Univ Chinese Acad Sci, 19 Yuquan Rd, Beijing 100049, Peoples R China
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GB/T 7714
Han, Fuzhou,Li, Geping,Yuan, Fusen,et al. A novel ultra-low current and temperature controlled electrochemical method for exposing various kinds of secondary phase precipitates: Application to the sample preparation of zirconium alloys and some other common alloys[J]. MATERIALS CHEMISTRY AND PHYSICS,2021,265:9.
APA Han, Fuzhou.,Li, Geping.,Yuan, Fusen.,Ali, Muhammad.,Zhang, Yingdong.,...&Gu, Hengfei.(2021).A novel ultra-low current and temperature controlled electrochemical method for exposing various kinds of secondary phase precipitates: Application to the sample preparation of zirconium alloys and some other common alloys.MATERIALS CHEMISTRY AND PHYSICS,265,9.
MLA Han, Fuzhou,et al."A novel ultra-low current and temperature controlled electrochemical method for exposing various kinds of secondary phase precipitates: Application to the sample preparation of zirconium alloys and some other common alloys".MATERIALS CHEMISTRY AND PHYSICS 265(2021):9.
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