IMR OpenIR
共晶Sn3.8Ag0.7Cu焊料合金在静态、单向、循环及力电加载下的形变与断裂
其他题名Deformation and Rupture of Eutectic Sn3.8Ag0.7Cu Solder Alloy under Static, Monotonic, Cyclic, and Electromechanical Loadings
张黎
学位类型博士
导师韩恩厚
2007-06-04
学位授予单位中国科学院金属研究所
学位授予地点金属研究所
学位专业材料物理与化学
关键词无铅焊料 共晶snagcu合金 静态蠕变 电迁移 循环蠕变 应力松弛 门槛应力
摘要在电子工业中,焊料广泛用于芯片与封装基体(印制电路板)的连接。一直以来,锡基含铅焊料凭借其优良的润湿性、高的可靠性以及低成本在电子封装领域广为使用。然而,随着社会对环境保护的日益关注,铅的使用受到很大的限制,美国、日本、欧盟已经开始从立法上对铅的使用进行明确的限制。因此,使用无铅焊料是微电子封装工业发展的必然趋势。与此同时,寻求新的可替代的无铅焊料就成了目前微电子封装工业的焦点。从当前的发展状况看,共晶SnAgCu合金最有可能代替SnPb合金。 在对无铅合金的筛选中,焊点的可靠性是一个至关重要的考虑方面,包括合金的抗蠕变性能、抗电迁移能力等。本论文从焊点合金的本身的力学性能着手,研究了冷却速率对共晶Sn3.8Ag0.7Cu合金微观组织的影响。在拉伸试验中,通过对不同应变速率下拉伸行为的研究,发现其最大拉伸强度具有应变速率敏感性,并利用微观颈缩过程对其形变过程进行了解释。静态蠕变和循环蠕变试验表明,这种合金具有较高的名义应力敏感指数,门槛应力的引入给予这种高的应力敏感指数合理解释。利用位错与粒子的交互作用的概念,解释了门槛应力的来源。激活能的计算表明,合金的蠕变机制与温度和应力相关。对静态蠕变而言,在低应力区,存在一个蠕变机制转换温度。但对循环蠕变来说,其蠕变机制的转换温度与加载应力区间无关,且其较静态蠕变的转换温度低。利用“非热空位模型”,可以给这种转变温度的降低较好的解释。此外,此模型也较好的解释了循环蠕变中的循环加速和循环减速现象。通过对蠕变断裂时间的参数法分析,Manson-Haferd 法可给出最好的拟合结果。 在对焊点结构的性能研究中,原位电迁移研究表明,小丘(hillock)在焊点表面出现,阴极界面化合物被消耗。此后的力学性能研究结果显示,电迁移过程严重弱化了焊点强度,分析表明这与电迁移过程引入的过多空位相关。焊点结构的断裂方式与加载的电流密度大小、通电时间有关,随着电迁移程度的加剧,有从延性断裂到脆性断裂的趋势。应力松弛试验结果表明,电迁移过程促使应力松弛速率增加,但并不改变松弛过程的蠕变机制。
其他摘要Solder is widely used to connect chips to their packaging substrates (e.g., print circuit board) in electronic industry. For a long time, Pb-containing Sn-based solder alloys were predominant in electronic packaging because of their excellent wetting property, high reliability and low cost. However, Pb presents potential health hazards so that their use in electronics must be minimized. To limit Pb use in electronics, US, Japan and EU have taken various legislative steps, including a complete ban of Pb-bearing solders in electronic products. In preparation for a complete ban, the electronic packaging industry has been actively searching for Pb-free replacement of Pb-bearing solders. Among many candidates, the eutectic Sn-Ag-Cu is emerging as the most promising replacement. For the selection of a suitable replacement, the reliability of the solder joint is a critical issue. The reliability concerns may arise from creep and electromigration of the solder alloy because of low melting temperature of Sn-based alloys. However, both the creep resistance and electromigration resistance of solder alloys were not well understood. In this study, deformation and rupture behavior of the eutectic Sn-Ag-Cu solder alloy was investigated under a range of mechanical and electromechanical loading conditions. Under monotonic loading, the strain rate sensitivity of ultimate tensile strength (UTS) was measured by changing the loading rates. The strain rate sensitivity was found to be relatedto micro-necking process. Under both static and cyclic loadings, the alloy exhibited higher creep stress exponents, which can be explained by the introduction of a threshold stress. The threshold stress was shown to arise from the interaction between dislocations and second phase particles. From the values of the creep activation energy, it was concluded that more than one creep mechanisms operated and the dominant creep mechanism in this solder alloy depended on applied stress and temperature. In the static creep, the dominant creep mechanism went through a transition in the low stress region. However, in the cyclic creep, the transition was independent of the applied stress and occurred at a lower temperature. The transitions were explained by athermal vacancy model, which also provided a good explanation for cyclic creep acceleration and retardation. Analysis of the creep rupture data indicated that the rupture time could be best analyzed by the Manson-Haferd method. Under electromechanical loading, the solder alloy showed severe softening and faster deformation rates. Application of electric loading before tensile tests resulted in significant weakening of the solder alloy and solder interface. Such a current-induced softening of the solder alloy was related to the excess vacancies generated by electromigration. With prolonged electrical loading, the rupture mode changed from ductile to brittle failure. The relaxation experiments showed that the stress relaxation rate after electromigration was higher than that of as-cast sample, but the creep activation energy was the same. Even faster deformation rates were found under combined electrical and mechanical loads.
页数157
语种中文
文献类型学位论文
条目标识符http://ir.imr.ac.cn/handle/321006/16952
专题中国科学院金属研究所
推荐引用方式
GB/T 7714
张黎. 共晶Sn3.8Ag0.7Cu焊料合金在静态、单向、循环及力电加载下的形变与断裂[D]. 金属研究所. 中国科学院金属研究所,2007.
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