IMR OpenIR
Mg-Er基非晶合金及其复合材料
其他题名Mg-Er based bulk amorphous alloys and their composites
刘文月
学位类型博士
导师张海峰
2007-05-19
学位授予单位中国科学院金属研究所
学位授予地点金属研究所
学位专业材料学
关键词Mg-er基非晶合金 玻璃形成能力 非晶形成尺寸计算 非晶基复合材料 过冷液相区 牛顿流体
摘要Mg基非晶合金因其高强度、低密度,作为新型高比强度结构材料具有广阔的应用前景。一般而言,大原子尺寸差与主要组元间具有负混合热的多组元体系,具有高的玻璃形成能力。但是,目前尚无任何理论或者方法可以量化合金成分与玻璃形成能力之间的关系。本文的主要目的就是探索这一量化关系,进而开发出新的Mg基非晶合金成分。 首先,通过分析现有典型合金体系玻璃形成能力与组元间的特点,利用组元的本征性质:电负性、价电子数、熔点、原子尺寸,建立了合金玻璃形成能力的计算模型。通过实验值与计算值之间的对比,该模型在计算玻璃形成能力方面,具有较高的精度,统计相关因子R2可达0.85。 再次,在模型计算的基础上,开发出了Mg-Er基非晶合金体系。通过模型分析与改进,能够较好的说明Mg-Cu-Er、Mg-Cu-Ag-Er合金系的玻璃形成能力与合金成分的关系。实验验证了计算模型的预测结果,计算与实验相结合有利于非晶合金成分开发工作的顺利进行。 随后,测试Mg-Er基非晶合金的室温力学性能发现,这类合金具有高强度、高硬度的特点,但是室温塑性变形量有限。通过复合技术,非晶材料的室温塑性明显提高,7v%Nbp-Mg60Cu30Er10合金的室温塑性可达5-6%。塑性提高的原因是添加Nb颗粒后诱发了剪切带萌生,促进了剪切带增殖,阻碍了剪切带自由扩展。 复合的方法虽然提高了塑性,但是未改变非晶基体高度局域化的变形方式,塑性加工仍是问题。为此研究了Mg60Cu30Er10非晶合金在过冷液相温区内的变形行为。研究发现,在此温区内合金可以进行低应力水平下(100MPa)大变形量(50-60%)的塑性变形,这为Mg-Er基非晶合金的塑性加工提供了出路。
其他摘要Mg-Er based bulk amorphous alloys and their composites W.Y. Liu (Materials Science) Supervised by Prof. H.F. Zhang, Vice Prof. A.M. Wang and Prof. Z.Q. Hu Mg based amorphous alloys are regarded as a new family of the promising structural materials for their high strength and low density. Generally, multi-component system shows good glass forming ability (GFA) which has the characters of large atomic size mismatch and negative mixing heat amongst the constituent elements. But no method or theory can solve the challenge of quantified relationship between alloy component and glass forming ability. In this paper, the main purpose is to build the quantified relationship and then to explore new Mg based bulk amorphous alloy system. Firstly, we build the model to calculate GFA of alloys, using the intrinsic material properties (atomic size, electro-negativity, melting point and valence electron of the constituent element), through analyzing the character of typical glass forming formers. Comparing with the experimental results, the model can be applied in GFA calculation successfully with high precision. The statistical correlation parameter R2 is as high as 0.85. Secondly, based on the GFA calculation model we developed a new Mg-Er based bulk amorphous alloy system. Through modification the GFA calculation model, the relationship between alloy constituents and its glass forming ability are clarified very well. Calculation values agree well with experimental values. With the guide of calculation model, exploring new amorphous alloy progress smoothly。 Thirdly, after testing their mechanical properties, the Mg-Er based amorphous alloys show high fracture strength and high micro-hardness, but plastic strain is limited at ambient temperature. In order to solve the problem, the Nb particles (Nbp) strengthened metallic glass matrix composites, Nbp-Mg60Cu30Er10 composites have been fabricated, which have high plastic strain values about 5-6%. The effect of Nbp is helpful of inducing to generate more shear bands, promoting their bifurcation and hindering their free propagation. Nbp-Mg60Cu30Er10 composites posses a certain amount of plastic strain, but their matrixes are still deformed by the mode of localized shear bands. Plastic shaping is still unsolved. So it is proposed to investigate the deformation behavior of Mg60Cu30Er10 amorphous alloy in the supercooled liquid region. The supercooled liquid can show remarkable homogeneous plastic strain (about 50-60%) with rather low flow stress (less than 100MPa). This property can help us to shaping Mg-Er based bulk amorphous alloys.
页数135
语种中文
文献类型学位论文
条目标识符http://ir.imr.ac.cn/handle/321006/17028
专题中国科学院金属研究所
推荐引用方式
GB/T 7714
刘文月. Mg-Er基非晶合金及其复合材料[D]. 金属研究所. 中国科学院金属研究所,2007.
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