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镁合金Mg-3Al-1Zn 及Mg-12Gd-3Y-0.5Zr 的低周疲劳行为
其他题名Low cycle fatigue behaviors of Mg-3Al-1Zn and Mg-12Gd-3Y-0.5Zr alloy
尹树明
学位类型博士
导师李守新
2009-01-08
学位授予单位中国科学院金属研究所
学位授予地点金属研究所
学位专业材料物理与化学
关键词镁合金 低周疲劳 织构 孪生-退孪生 拉-压屈服非对称性 循环硬化 循环软化 背散射电子衍射 等通道转角挤压
摘要镁合金具有密度低、比刚度、比强度高等优点,在节能减重等方面很有吸引力。目前,研发镁合金已列入国家 “十一五”发展规划。近年来,随着镁合金作为结构材料在实际应用的日益增多,对镁合金的疲劳性能的研究就显得非常必要。然而,目前对镁合金的疲劳性能的了解还不够深入,尤其是镁合金的织构及孪晶对其疲劳行为的影响还不清楚;对于一些新研制的镁合金,目前对其基本的疲劳性能知之甚少。 本文选择商用挤压镁合金AZ31 (Mg‐3%Al‐1%Zn wt.%)棒材,研究其室温恒塑性应变控制下的低周疲劳行为,旨在研究织构及孪晶对此类镁合金低周疲劳性能的影响;选择新型镁合金GW123K (Mg‐12%Gd‐3%Y‐0.5%Zr wt.%)为研究对象,主要考察其室温总应变控制下基本的疲劳性能。此外,对上述两种镁合金进行一道次ECAP 处理,研究对应的拉伸、压缩及疲劳性能,主要结论如下: 1. 对常规挤压态镁合金AZ31 的室温拉伸和压缩性能研究表明,该材料存在较大的拉压屈服非对称性,压缩屈服强度还不及拉伸屈服强度的一半,这主要是由于在挤压过程中形成很强的{0002} < 1120 > 丝织构,压缩屈服过时拉伸孪生是主要的塑性变形方式,拉伸屈服过程中柱面滑移是主要的变形方式,因二者开动所需的应力相差较大,从而产生较大的拉‐压屈服非对称性。 2. EBSD 原位观察证实了AZ31 挤压棒材在轴向压‐拉循环加载过程中的微观变形方式是孪生‐退孪生。 3. 常规挤压态镁合金AZ31 棒材表现出循环硬化非对称性,拉伸半周硬化速率明显高于压缩半周的硬化速率;从滞后回线上还可以发现伪弹性、为塑性及拉压屈服非对称性,其主要原因是在循环加载过程中发生了孪生与退孪生。 4. 常规挤压态耐热镁合金总应变控制下GW123K 合金表现出循环稳定,裂纹萌生于大尺寸的夹杂物或者是富钆的第二相处。 5. 经过一道次ECAP 处理,由于晶粒的细化和初始织构的弱化使镁合金AZ31 的拉压屈服非对称性显著降低,对应的疲劳寿命略有提高;一道次ECAP 处理可以使GW123K 的拉伸塑性得到显著提高,合金在疲劳过程中仍保持循环稳定,又能使其应变疲劳寿命保持住原有的水平。
其他摘要Study and develop magnesium alloys is one aspect of the outline of China's the Eleventh Five-year Plan. Magnesium (Mg) alloys are very attractive materials in order to achieve high performance and energy saving of machines and structures, because of their advantages such as light weight, high strength-to-weight ratio and high specific stiffness. Therefore, they have recently been increasing interest as tructural materials in many applications. For applications to load-bearing components, it is necessary to evaluate fatigue properties. However, there have been limited studies on the influence of texture and twin on fatigue behavior of magnesium alloy. Besides, the basic fatigue properties of some new developed magnesium alloys are unknown at present. In the present study, axial plastic strain controlled fatigue tests have been performed using smooth specimens of a conventional extruded AZ31 Mg alloy in laboratory air at ambient temperature with an aim to study the influence of texture and twin on fatigue behavior of magnesium alloy; Total strain controlled fatigue tests performed using extruded Mg-12Gd-3Y-0.5Zr (GW123K) in order to know the basic fatigue behavior of the new developed magnesium alloy. In this dissertation, low cycle fatigue behaviors of single pass equal channel angular pressed (ECAP) magnesium alloy AZ31 and Mg-12Gd-3Y-0.5Zr (GW123K) also investigated. The main results are as follows: 1. Conventional extruded AZ31 with strong fiber texture exhibits large tension-compression yield asymmetry. The ratio of yield stress between compression and tension less than 0.5 which result from different micro-deformation mechanism. It is believed that tension twinning dominates deformation in compression and the stress needed to activate tension twinning less than the stress needed to activate prism slip which dominates deformation in tension when loading along extruded direction. 2. EBSD in-situ observation shows clearly that twinning-detwinning operate alternately during fatigue. 3. The conventional extruded AZ31 exhibits cyclic hardening asymmetry that the compressive stress amplitude increased slightly while tensile stress amplitude increased significantly with the number of cycles increasing. Besides, pesudo-elastic and pesudo-plastic behavior as well as yield asymmetry were found on the hysteresis loop. These behaviors are result from twinning-detwining during fatigue. 4. The conventional extruded GW123K (Mg-12%Gd-3%Y-0.5%Zr) alloy maintained cyclic stability during most of the cycling times. Fracture morphology observation indicated that cracks initiated at large Gd-rich regions as well as inclusions at surface or subsurface. 5. The yield asymmetry of AZ31 processed by ECAP for single pass decreased significantly which result from the weakened fiber texture and grain size refining. The fatigue life of ECAPed AZ31 alloy increased slightly. For GW123K alloy, after one passes of ECAP, the ductility of the alloy increased significantly. The ECAPed GW123K alloy maintains cyclic stability during fatigue and the fatigue life of the material keep the same level as the initial state.
页数105
语种中文
文献类型学位论文
条目标识符http://ir.imr.ac.cn/handle/321006/17055
专题中国科学院金属研究所
推荐引用方式
GB/T 7714
尹树明. 镁合金Mg-3Al-1Zn 及Mg-12Gd-3Y-0.5Zr 的低周疲劳行为[D]. 金属研究所. 中国科学院金属研究所,2009.
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