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离子注入对多晶镍微观结构及疲劳行为的影响
徐明华
学位类型硕士
导师王中光
1988
学位授予单位中国科学院金属研究所
学位授予地点中国科学院金属研究所
摘要本文研究了 C~+、N~+注入前后,多晶镍的疲劳行为,同时利用俄歇能谱仪、扫描电镜和透射电镜等研究了疲劳前后,未注入和C~+或N~+注入试样表面层的微观结构。分析了离子注入影响疲劳寿命的可能原因。实验结果表明N~+、C~+注入分别使镍的疲劳极限提高了 21%和25%。比较未注入试样,离子注入过试样的表面出现滑移带的晶粒数目明显减少,滑移带变细,表面比较平坦。未注入试样的疲劳裂纹沿滑移带萌生,而 N~+ 注入后,裂纹在晶界萌生。经 C~+ 注入后,晶界和滑移带都萌生裂纹。C~+ 注入导致Ni表面层非晶化,而疲劳的作用促使非晶层晶化。在综合分析实验结果的基础上,提出了离子注入改善疲劳性能的可能原因。在N~+ 注入的情况归结于表面压应力,固容强化以及堆垛层错能的降低,而C~+ 的注入则是通过形成非晶层和使晶粒细化提高疲劳寿命。
其他摘要In this paper, pure polycrystalline nickel with and without nitrgen (carbon) ion implantation has been fatigued. Surface layer microstructure of specimens with and without ion implantation, before and after fatigue, has been examined with AES, SEM and TEM. The reason why ion implantation influences fatigue life has been discussed. The experiment results show that the endurance limit of pure nickel with N~+ (C~+) implantation increases by 21% (25%). Compared with that of unimplanted specimens, the number of surface grains, in which slip bands could be found, decreases, slip bands become finer and specimen surface is still smooth after the implanted specimens were fatigued. Slip band cracking which is found in the unimplanted specimens is replaced by grain boundary cracking in N~+ implantation specimens, the two modes of crack initiation could be found in C~+ implantation specimens. It has been found that nickel surface layer is amorphized by carbon ion implantation, amorphous layer is crystallized in course of fatigue. Based on the analysis of experiment results, it is considered that the improvement in fatigue life by nitrogen ion implantation is attributed to the surface compressive stress, solid solution strengthen and lowering stacking fault energy; the increase of fatigue life of carbon-implanted specimens is because of forms of amorphous layer and fine grains.
页数66
语种中文
文献类型学位论文
条目标识符http://ir.imr.ac.cn/handle/321006/17358
专题中国科学院金属研究所
推荐引用方式
GB/T 7714
徐明华. 离子注入对多晶镍微观结构及疲劳行为的影响[D]. 中国科学院金属研究所. 中国科学院金属研究所,1988.
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