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定向凝固气冷叶片用陶瓷型芯高温特性的研究
王景周
学位类型硕士
导师胡壮麒
1989
学位授予单位中国科学院金属研究所
学位授予地点中国科学院金属研究所
摘要用30%的锆英石和70%的石英玻璃制成的定向凝固气冷叶片用陶瓷型芯,不但具有高的耐火度和强度,良好的化学稳定性和尺寸精度,而且具备易于从铸件中脱除等优点。本文首先测试了该型芯试样在1200-1600 ℃内的高温变形,抗弯强度,收缩率和溶蚀性的变化规律,然后借助X光衍射、扫描电镜、电子探针及金相分析等手录。对其变化规律进行了分析。结果发现,在1200-1600 ℃温区内,收缩率随温度的升高而增大和溶蚀速度随温度的升高而减小,主要与型芯的粘滞流动有关。随着温度的升高和粘滞流动的发生,型芯的微观相之间的孔隙逐渐变小,收缩率就增大,同时由于气孔率下降,降低了型芯与溶蚀液之间的接触面积,所以溶蚀速度就减小。高温变形量在1550 ℃左右有一个激增,主要与Al_2O_3和SiO_2结合形成液相有关。抗弯强度值在1350-1400 ℃之间发生突降,主要与石英玻璃的大量析晶有关。此外, 本文还分析了在延长保温时间的条件下,型芯的性能变化与微观组织的变化之间的关系。
其他摘要The silica-base core for directionally solidified air-cooled blade and vane is composed of 30% zirconia and 70% quartz. Not only its refractoriness and strength are high as well as its chemistry stability and size precision are excellent, but also it can be removed easily. The high temperature deformation, bending strength, contraction and corroision rate of the core specimens were measured in the temperature range of 1200-1600 ℃, that were studied in detail by means of x-ray diffraction, scanning electron microscope, electron microprobe analysis and metallographic analysis. The results show that with the rise of temperature the contraction rate increases but the corrosion rate decreases mainly due to the variation of the viscous flow of core. The gap between the particles of core decreases, that makes the contraction rate increase. Because of the drop of microporosity, the contact area between core and corrosive liquid decreases. Therefore, corrosion rate becomes slower gradually. The dramatic increases of high temperature deformation around 1550 ℃ is mainly resulted from the formation of liquid phase (compound of Al_2O_3 and SiO_2). The remarkable impairment of bending strength between 1350-1400 ℃ is mainly due to a great deal of quartz transferring into crystalline state. Besides, the change of properties of core was studied in the condition of prolonged soaking at high temperature.
页数58
语种中文
文献类型学位论文
条目标识符http://ir.imr.ac.cn/handle/321006/17417
专题中国科学院金属研究所
推荐引用方式
GB/T 7714
王景周. 定向凝固气冷叶片用陶瓷型芯高温特性的研究[D]. 中国科学院金属研究所. 中国科学院金属研究所,1989.
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