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Highly efficient nickel fluoride nanoparticles with enhance electrochemical properties
Soomro, Faheeda1; Khan, Jamshid2; Ullah, Sami3; Abutaleb, Ahmed4; Zouli, Nasser4; Iqbal, Muzaffar5; Sajjad, Muhammad6; Khan, Firoz7; HussainThebo, Khalid8
通讯作者Zouli, Nasser(nizouli@jazanu.edu.sa) ; Iqbal, Muzaffar(muzaffar.iqbal@uoh.edu.pk) ; HussainThebo, Khalid(khalidthebo@yahoo.com)
2023-09-01
发表期刊INORGANIC CHEMISTRY COMMUNICATIONS
ISSN1387-7003
卷号155页码:8
摘要Due to their unique physical and chemical characteristics, nanostructured materials of various architectures have demonstrated tremendous promise in the fields of energy and the environment. In this study, the reverse micellar emulsion approach is used to prepare cubic NiF2 nanoparticles (NPs) in order to produce self-assembled NiF2 nanostructures with a certain morphology. Hydrated and anhydrous NiF2 NPs are prepared by studying the key reaction parameters, such as changing water to surfactant (sodium dodecyl sulfate) ratio, synthesis temperature, and the amount of solvent (cyclohexanol). The hydrated NiF2 NPs were sintered at 400 degrees C for 3 h under nitrogen gas at 5.0 mbar pressure to achieve the anhydrous NiF2 NPs. The X-ray diffraction (XRD) studies reveal the tetragonal crystal structure with a crystallite size of 60 to 77 nm. While scanning electron microscopy (SEM) studies show the cubic morphology of as-prepared NiF2 NPs. The cyclic voltammetry was performed to determine oxidation/reduction, current, and reversibility of both anhydrous and hydrated NiF2 NPs. The cyclic voltammetry result shows that the electrochemical activities of sintered NiF2 NPs were greatly improved up to similar to 0.9 Ah because of their structures, morphology, and size compared to pre-sintering NPs.
关键词Nickel fluoride Nanoparticles Micro-emulsion Electrochemical activity Sodium dodecyl sulfate
资助者Deputyship for research amp; innovation, Ministry of Education in Saudi Arabia
DOI10.1016/j.inoche.2023.111023
收录类别SCI
语种英语
资助项目Deputyship for research amp; innovation, Ministry of Education in Saudi Arabia[ISP22-4]
WOS研究方向Chemistry
WOS类目Chemistry, Inorganic & Nuclear
WOS记录号WOS:001041003200001
出版者ELSEVIER
引用统计
被引频次:12[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://ir.imr.ac.cn/handle/321006/178859
专题中国科学院金属研究所
通讯作者Zouli, Nasser; Iqbal, Muzaffar; HussainThebo, Khalid
作者单位1.Begum Nusrat Bhutto Women Univ, Dept Linguist & Human Sci, Rohri Bypass, Sukkur, Sindh, Pakistan
2.Hazara Univ, Dept Chem, Mansehra 21300, Pakistan
3.King Fahd Univ Petr & Minerals KFUPM, KA CARE Energy Res & Innovat Ctr ERIC, Dhahran 31261, Saudi Arabia
4.Jazan Univ, Coll Engn, Dept Chem Engn, POB 706, Jazan 45142, Saudi Arabia
5.Univ Haripur, Fac Phys & Appl Sci, Dept Chem, KPK 22620, Pakistan
6.Kohat Univ Sci & Technol, Dept Phys, Kohat 26000, Pakistan
7.King Fahd Univ Petr & Minerals KFUPM, Interdiscipliary Res Ctr Renewable Energy & Power, Dhahran 31261, Saudi Arabia
8.Chinese Acad Sci, Inst Met Res, 72 Wenhua Rd, Shenyang 110016, Peoples R China
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GB/T 7714
Soomro, Faheeda,Khan, Jamshid,Ullah, Sami,et al. Highly efficient nickel fluoride nanoparticles with enhance electrochemical properties[J]. INORGANIC CHEMISTRY COMMUNICATIONS,2023,155:8.
APA Soomro, Faheeda.,Khan, Jamshid.,Ullah, Sami.,Abutaleb, Ahmed.,Zouli, Nasser.,...&HussainThebo, Khalid.(2023).Highly efficient nickel fluoride nanoparticles with enhance electrochemical properties.INORGANIC CHEMISTRY COMMUNICATIONS,155,8.
MLA Soomro, Faheeda,et al."Highly efficient nickel fluoride nanoparticles with enhance electrochemical properties".INORGANIC CHEMISTRY COMMUNICATIONS 155(2023):8.
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