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Joining of Ti(3)SiC(2) by Magnetron Sputtering a Layer of Cu or Zr Followed by Heat Treating at Relatively Low Temperatures
A. J. Li; Y. C. Zhou
2011
发表期刊Journal of the American Ceramic Society
ISSN0002-7820
卷号94期号:9页码:3072-3077
摘要Ti(3)SiC(2) joining has been successfully achieved by depositing a thin Cu or Zr layer on it and heat treating at low temperatures of 950 degrees or 1100 degrees C in an argon atmosphere, respectively, which are similar to 500 degrees C lower than the previous solid solution joining method. X-ray diffraction and scanning electron microscope analyses reveal that a continuous Cu(3)Si or Zr-silicide layer forms at the joint interface through the outward diffusion of Si atoms from the Ti(3)SiC(2) substrate into the deposited Cu or Zr layer. The strength of joints is evaluated by tensile bond-strength test and 4-point bending test methods. The Ti(3)SiC(2)/Cu/Ti(3)SiC(2) joints always fail from the substrate instead of from the bonding interface, while the Ti(3)SiC(2)/Zr/Ti(3)SiC(2) joints fail from the joint interface during tensile bond-strength test. The 4-point bending strength of Ti(3)SiC(2)/Cu/Ti(3)SiC(2) joints reaches a value of 238 MPa, which is 68% of the Ti(3)SiC(2) substrate. So joining using a Cu or Zr film as the interlayer followed by heat treating is a practical and efficient method for joining Ti(3)SiC(2).
部门归属[li, aijun; zhou, yanchun] chinese acad sci, shenyang natl lab mat sci, inst met res, shenyang 110016, peoples r china. [li, aijun] chinese acad sci, grad sch, beijing 100039, peoples r china.;zhou, yc (reprint author), amer ceram soc, westerville, oh 43082 usa;yczhou714@gmail.com
关键词Interfacial Reactions Mechanical-properties Damage Tolerance Bulk Ceramics Thin-films Oxidation Microstructure Strength (111)Si Air
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文献类型期刊论文
条目标识符http://ir.imr.ac.cn/handle/321006/30445
专题中国科学院金属研究所
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A. J. Li,Y. C. Zhou. Joining of Ti(3)SiC(2) by Magnetron Sputtering a Layer of Cu or Zr Followed by Heat Treating at Relatively Low Temperatures[J]. Journal of the American Ceramic Society,2011,94(9):3072-3077.
APA A. J. Li,&Y. C. Zhou.(2011).Joining of Ti(3)SiC(2) by Magnetron Sputtering a Layer of Cu or Zr Followed by Heat Treating at Relatively Low Temperatures.Journal of the American Ceramic Society,94(9),3072-3077.
MLA A. J. Li,et al."Joining of Ti(3)SiC(2) by Magnetron Sputtering a Layer of Cu or Zr Followed by Heat Treating at Relatively Low Temperatures".Journal of the American Ceramic Society 94.9(2011):3072-3077.
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