摘要 | Yttrium aluminum garnet (YAG) precursor was prepared by sol-gel combustion method using ethanol as solvent. Nano-sized YAG powders were obtained by precalcining the precursor at 500 degrees C, and then calcining at different temperatures. The phase formation and characteristics of YAG powders were investigated by means of XRD, TG/DSC and TEM. Pure crystalline YAG phase was obtained at 800 degrees C, without any intermediate phases such as YAlO(3) (YAP) and Y(4)Al(2)O(9) (YAM). Moreover, it was found that the elliptical YAG powder calcined at 900 degrees C for 2 h was well-crystallized with an average size of 30 nm, and had a good dispersity. (C) 2009 Elsevier B.V. All rights reserved.; Yttrium aluminum garnet (YAG) precursor was prepared by sol-gel combustion method using ethanol as solvent. Nano-sized YAG powders were obtained by precalcining the precursor at 500 degrees C, and then calcining at different temperatures. The phase formation and characteristics of YAG powders were investigated by means of XRD, TG/DSC and TEM. Pure crystalline YAG phase was obtained at 800 degrees C, without any intermediate phases such as YAlO(3) (YAP) and Y(4)Al(2)O(9) (YAM). Moreover, it was found that the elliptical YAG powder calcined at 900 degrees C for 2 h was well-crystallized with an average size of 30 nm, and had a good dispersity. (C) 2009 Elsevier B.V. All rights reserved.; Yttrium aluminum garnet (YAG) precursor was prepared by sol-gel combustion method using ethanol as solvent. Nano-sized YAG powders were obtained by precalcining the precursor at 500 degrees C, and then calcining at different temperatures. The phase formation and characteristics of YAG powders were investigated by means of XRD, TG/DSC and TEM. Pure crystalline YAG phase was obtained at 800 degrees C, without any intermediate phases such as YAlO(3) (YAP) and Y(4)Al(2)O(9) (YAM). Moreover, it was found that the elliptical YAG powder calcined at 900 degrees C for 2 h was well-crystallized with an average size of 30 nm, and had a good dispersity. (C) 2009 Elsevier B.V. All rights reserved. |
部门归属 | [lu, tiecheng] sichuan univ, minist educ, dept phys, key lab radiat phys & technol, chengdu 610064, peoples r china. [lu, tiecheng] chinese acad sci, int ctr mat phys, shenyang 110015, peoples r china. [xu, hui] sipo, patent examinat cooperat ctr, beijing 100190, peoples r china.;lu, tc (reprint author), sichuan univ, minist educ, dept phys, key lab radiat phys & technol, chengdu 610064, peoples r china;lutiecheng@vip.sina.com
; [lu, tiecheng] sichuan univ, minist educ, dept phys, key lab radiat phys & technol, chengdu 610064, peoples r china. [lu, tiecheng] chinese acad sci, int ctr mat phys, shenyang 110015, peoples r china. [xu, hui] sipo, patent examinat cooperat ctr, beijing 100190, peoples r china.;lu, tc (reprint author), sichuan univ, minist educ, dept phys, key lab radiat phys & technol, chengdu 610064, peoples r china;lutiecheng@vip.sina.com
; [lu, tiecheng] sichuan univ, minist educ, dept phys, key lab radiat phys & technol, chengdu 610064, peoples r china. [lu, tiecheng] chinese acad sci, int ctr mat phys, shenyang 110015, peoples r china. [xu, hui] sipo, patent examinat cooperat ctr, beijing 100190, peoples r china.;lu, tc (reprint author), sichuan univ, minist educ, dept phys, key lab radiat phys & technol, chengdu 610064, peoples r china;lutiecheng@vip.sina.com
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推荐引用方式 GB/T 7714 |
L. Yang,T. C. Lu,H. Xu,et al. Synthesis of YAG powder by the modified sol-gel combustion method, Synthesis of YAG powder by the modified sol-gel combustion method, Synthesis of YAG powder by the modified sol-gel combustion method[J]. Journal of Alloys and Compounds, Journal of Alloys and Compounds, Journal of Alloys and Compounds,2009, 2009, 2009,484, 484, 484(1-2):449-451, 449-451, 449-451.
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