Low-temperature synthesis and sintering of gamma-Y2Si2O7 | |
Z. Q. Sun; Y. C. Zhou; M. S. Li | |
2006 | |
发表期刊 | Journal of Materials Research
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ISSN | 0884-2914 |
卷号 | 21期号:6页码:1443-1450 |
摘要 | In this article, a novel pressureless solid-liquid reaction method is presented for preparation of yttrium disilicate (gamma-Y2Si2O7). Single-phase gamma-Y2Si2O7 powder was synthesized by calcination of SiO2 and Y2O3 powders with the addition of LiYO2 at 1400 degrees C for 4 h. The addition of LiYO2 significantly decreased the synthesis temperature, shortened the calcination time, and enhanced the stability of gamma-Y2Si2O7. The sintering of these powders in air and O-2 was studied by means of thermal mechanical analyzer. It is shown that the gamma-Y2Si2O7 sintered in oxygen had a faster densification rate and a higher density than that sintered in air. Furthermore, single-phase gamma-Y2Si2O7 with a density of 4.0 g/cm(3) (99% of the theoretical density) was obtained by pressureless sintering at 1400 degrees C for 2 h in oxygen. Microstructures of the sintered samples are studied by scanning electron microscope. |
部门归属 | chinese acad sci, high performance ceram div, shenyang natl lab mat sci, inst met res, shenyang 110016, peoples r china. chinese acad sci, grad sch, beijing 100039, peoples r china.;zhou, yc (reprint author), chinese acad sci, high performance ceram div, shenyang natl lab mat sci, inst met res, shenyang 110016, peoples r china;yczhou@imr.ac.cn |
关键词 | Yttrium Disilicate Powder Pressed Silicon-nitride Gel Method Behavior Crystallization Microstructure Densification Stability Evolution Ceramics |
URL | 查看原文 |
WOS记录号 | WOS:000238191300013 |
引用统计 | |
文献类型 | 期刊论文 |
条目标识符 | http://ir.imr.ac.cn/handle/321006/34479 |
专题 | 中国科学院金属研究所 |
推荐引用方式 GB/T 7714 | Z. Q. Sun,Y. C. Zhou,M. S. Li. Low-temperature synthesis and sintering of gamma-Y2Si2O7[J]. Journal of Materials Research,2006,21(6):1443-1450. |
APA | Z. Q. Sun,Y. C. Zhou,&M. S. Li.(2006).Low-temperature synthesis and sintering of gamma-Y2Si2O7.Journal of Materials Research,21(6),1443-1450. |
MLA | Z. Q. Sun,et al."Low-temperature synthesis and sintering of gamma-Y2Si2O7".Journal of Materials Research 21.6(2006):1443-1450. |
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