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Synthesis and characterization of double-walled carbon nanotubes from multi-walled carbon nanotubes by hydrogen-arc discharge
L. X. Li; F. Li; C. Liu; H. M. Cheng
2005
Source PublicationCarbon
ISSN0008-6223
Volume43Issue:3Pages:623-629
AbstractDouble-walled carbon nanotubes (DWNTs) were synthesized in a large scale by a hydrogen arc discharge method using graphite powders or multi-walled carbon nanotubes/carbon nanofibers (MWNTs/CNFs) as carbon feedstock. The yield of DWNTs reached about 4g/h. We found that the DWNT product synthesized from MWNTs/CNFs has higher purity than that from graphite powders. The results from high-resolution transmission electron microscopy observations revealed that more than 80% of the carbon nanotubes were DWNTs and the rest were single-walled carbon nanotubes (SWNTs), and their outer and inner diameters ranged from 1.75 to 4.87nm and 1.06 to 3.93nm, respectively. It was observed that the ends of the isolated DWNTs were uncapped and it was also found that cobalt as the dominant composition of the catalyst played a vital role in the growth of DWNTs by this method. In addition, the pore structures of the DWNTs obtained were investigated by cryogenic nitrogen adsorption measurements. (C) 2004 Elsevier Ltd. All rights reserved.
description.departmentchinese acad sci, met res inst, shenyang natl lab mat sci, shenyang 110016, peoples r china.;cheng, hm (reprint author), chinese acad sci, met res inst, shenyang natl lab mat sci, 72 wenhua rd, shenyang 110016, peoples r china;cheng@imr.ac.cn
KeywordCarbon Nanotubes Arc Discharge Adsorption Properties Microstructure Raman-scattering Catalytic Decomposition Diameter Distribution Fullerenes Identification Morphology
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WOS IDWOS:000226574600020
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Cited Times:59[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.imr.ac.cn/handle/321006/34901
Collection中国科学院金属研究所
Recommended Citation
GB/T 7714
L. X. Li,F. Li,C. Liu,et al. Synthesis and characterization of double-walled carbon nanotubes from multi-walled carbon nanotubes by hydrogen-arc discharge[J]. Carbon,2005,43(3):623-629.
APA L. X. Li,F. Li,C. Liu,&H. M. Cheng.(2005).Synthesis and characterization of double-walled carbon nanotubes from multi-walled carbon nanotubes by hydrogen-arc discharge.Carbon,43(3),623-629.
MLA L. X. Li,et al."Synthesis and characterization of double-walled carbon nanotubes from multi-walled carbon nanotubes by hydrogen-arc discharge".Carbon 43.3(2005):623-629.
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