Synthesis and characterization of Fe-Cl boracite

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	Synthesis and characterization of Fe-Cl boracite
	Z. H. Wang; D. Y. Geng; D. Li; X. G. Zhao; Z. D. Zhang; Y. P. Wang; J. M. Liu
	2001
发表期刊	Journal of Alloys and Compounds
ISSN	0925-8388
卷号	329 期号:1-2 页码:278-284
摘要	The Fe-Cl boracite is prepared by a procedure, consisting of solution mixing, heating, grinding and H-2 reduction. The high valence metal ion Fe3+ reacts with H-2 to form the low valence metal ion Fe3+ so that the corresponding boracite can be synthesized. The lattice parameters and the phase transition temperatures are determined by means of X-ray diffraction, transmission electron microscopy and differential scanning calorimetry. The hydrogen not only plays a role in reduction, but also prevents the oxidation of the mixture. The ferroelectric property at room temperature of the sample has been substantially demonstrated. (C) 2001 Elsevier Science BY All rights reserved.
部门归属	acad sinica, inst met res, shenyang 110015, peoples r china. nanjing univ, solid state microstruct lab, nanjing 210093, peoples r china.;zhang, zd (reprint author), acad sinica, inst met res, wenhua rd 72, shenyang 110015, peoples r china
关键词	Transition Metal Compounds Chemical Synthesis Tem Ferroelectric Chromium-chlorine Boracite Phase-transitions Cr3b7o13cl
URL	查看原文
WOS记录号	WOS:000171818000043
引用统计	被引频次：4[WOS] [WOS记录] [WOS相关记录]
文献类型	期刊论文
条目标识符	http://ir.imr.ac.cn/handle/321006/36837
专题	中国科学院金属研究所
推荐引用方式 GB/T 7714	Z. H. Wang,D. Y. Geng,D. Li,et al. Synthesis and characterization of Fe-Cl boracite[J]. Journal of Alloys and Compounds,2001,329(1-2):278-284.
APA	Z. H. Wang.,D. Y. Geng.,D. Li.,X. G. Zhao.,Z. D. Zhang.,...&J. M. Liu.(2001).Synthesis and characterization of Fe-Cl boracite.Journal of Alloys and Compounds,329(1-2),278-284.
MLA	Z. H. Wang,et al."Synthesis and characterization of Fe-Cl boracite".Journal of Alloys and Compounds 329.1-2(2001):278-284.