| Microstructure of Ti3SiC2 prepared by the in-situ hot pressing/solid-liquid reaction process; Microstructure of Ti3SiC2 prepared by the in-situ hot pressing/solid-liquid reaction process | |
| Y. C. Zhou; Z. M. Sun; B. H. Yu | |
| 2000 ; 2000 | |
| Source Publication | Zeitschrift Fur Metallkunde
 ; Zeitschrift Fur Metallkunde
|
| ISSN | 0044-3093 ; 0044-3093 |
| Volume | 91Issue:11Pages:937-941 |
| Abstract | The microstructure of Ti3SiC2 ceramic prepared by the in-situ hot pressing/solid-liquid reaction process was investigated by transmission electron microscopy. TiC and SiC were identified to be the main impurity phases in this material. The presence of TIC inclusions in Ti3SiC2 resulted in high density of dislocations within Ti3SiC2 matrix and even interfacial cracking. The SiC impurities were one-dimensional disordered, i.e. with overwhelming of stacking faults and could be distinguished from TiC. Beside the observed impurities imbedded in Ti3SiC2, an interesting phenomenon was that needle-shaped Ti3SiC2 was also observed within TiC grains. The needle-shape Ti3SiC2 grew in TIC following the crystallographic relations of (111) TiC // (0001) Ti3SiC2, (002) TiC // (1(1) over bar 04) Ti3SiC2, and [1(1) over bar0] TiC // [110] Ti3SiC2. Slip trace of basal plane dislocations were observed in Ti3SiC2 and the dislocations pile up at grain boundaries suggesting that significant plastic deformation would be expected in single crystal or coarse-grain material.; The microstructure of Ti3SiC2 ceramic prepared by the in-situ hot pressing/solid-liquid reaction process was investigated by transmission electron microscopy. TiC and SiC were identified to be the main impurity phases in this material. The presence of TIC inclusions in Ti3SiC2 resulted in high density of dislocations within Ti3SiC2 matrix and even interfacial cracking. The SiC impurities were one-dimensional disordered, i.e. with overwhelming of stacking faults and could be distinguished from TiC. Beside the observed impurities imbedded in Ti3SiC2, an interesting phenomenon was that needle-shaped Ti3SiC2 was also observed within TiC grains. The needle-shape Ti3SiC2 grew in TIC following the crystallographic relations of (111) TiC // (0001) Ti3SiC2, (002) TiC // (1(1) over bar 04) Ti3SiC2, and [1(1) over bar0] TiC // [110] Ti3SiC2. Slip trace of basal plane dislocations were observed in Ti3SiC2 and the dislocations pile up at grain boundaries suggesting that significant plastic deformation would be expected in single crystal or coarse-grain material. |
| description.department | chinese acad sci, inst met res, ceram & composite dept, shenyang 110015, peoples r china.;zhou, yc (reprint author), chinese acad sci, inst met res, ceram & composite dept, 72 wenhua rd, shenyang 110015, peoples r china ; chinese acad sci, inst met res, ceram & composite dept, shenyang 110015, peoples r china.;zhou, yc (reprint author), chinese acad sci, inst met res, ceram & composite dept, 72 wenhua rd, shenyang 110015, peoples r china |
| Keyword | Silicon-carbide Silicon-carbide Damage Damage Ceramics Ceramics Defects Defects |
| URL | 查看原文 ; 查看原文 |
| WOS ID | WOS:000166064000010 ; WOS:000166064000010 |
| Citation statistics | |
| Document Type | 期刊论文 |
| Identifier | http://ir.imr.ac.cn/handle/321006/37303 |
| Collection | 中国科学院金属研究所 |
| Recommended Citation GB/T 7714 | Y. C. Zhou,Z. M. Sun,B. H. Yu. Microstructure of Ti3SiC2 prepared by the in-situ hot pressing/solid-liquid reaction process, Microstructure of Ti3SiC2 prepared by the in-situ hot pressing/solid-liquid reaction process[J]. Zeitschrift Fur Metallkunde, Zeitschrift Fur Metallkunde,2000, 2000,91, 91(11):937-941, 937-941. |
| APA | Y. C. Zhou,Z. M. Sun,&B. H. Yu.(2000).Microstructure of Ti3SiC2 prepared by the in-situ hot pressing/solid-liquid reaction process.Zeitschrift Fur Metallkunde,91(11),937-941. |
| MLA | Y. C. Zhou,et al."Microstructure of Ti3SiC2 prepared by the in-situ hot pressing/solid-liquid reaction process".Zeitschrift Fur Metallkunde 91.11(2000):937-941. |
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