Comparison of the thermomagnetic and thermal effects during nanocrystallization of amorphous Fe76.5-xCu1NbxSi13.5B9 alloys | |
B. Varga; J. Takacs; A. Lovas; P. Kamasa; F. Zhou; J. Vandlik | |
1998 | |
发表期刊 | Journal of Materials Science & Technology
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ISSN | 1005-0302 |
卷号 | 14期号:4页码:323-326 |
摘要 | The results of thermomagnetic (TM) and calorimetric (DSC) measurements have been compared in order to clarify some details of the mechanism of nanophase-formation from Finemet-type precursors with different Nb contents. It was found that the main features of the DSC thermograms (shape, relative separation and amplitude of the exothermic peaks characteristic for the precipitation of the Fe-(Si) solid solution and the transition metal borides) depend mainly on the composition of the precursor glass, and are only slightly affected by the heating rate between 20 and 80 K/min. The amplitude of the uprise of the magnetization in the TM curves (attributed to the precipitation of bcc-Fe(Si) and borides) decreases with increasing Nb-content. The Curie-temperature of the precursor glasses, T-c(am(1)), the remainder amorphous phases, T-c(am(2)) and the bcc nanophase, T-c(n-Fe) are determined from the thermomagnetic curves. The shape of the TM curves is interpreted on the basis of the reactions describing the crystallization of the hypo-eutectic Fe-B glasses. |
部门归属 | tech univ budapest, dept mech engn technol, h-1111 budapest, hungary. hungarian acad sci, solid state phys res inst, h-1525 budapest, hungary. chinese acad sci, inst met res, state key lab rsa, shenyang 110015, peoples r china. hungarian acad sci, inst sci mat, h-1525 budapest, hungary.;varga, b (reprint author), tech univ budapest, dept mech engn technol, bertalan l utca 2, h-1111 budapest, hungary |
关键词 | Thermodynamic Functions Association Model Liquid Alloys Crystallization Temperature |
URL | 查看原文 |
WOS记录号 | WOS:000074996700007 |
引用统计 | |
文献类型 | 期刊论文 |
条目标识符 | http://ir.imr.ac.cn/handle/321006/37796 |
专题 | 中国科学院金属研究所 |
推荐引用方式 GB/T 7714 | B. Varga,J. Takacs,A. Lovas,et al. Comparison of the thermomagnetic and thermal effects during nanocrystallization of amorphous Fe76.5-xCu1NbxSi13.5B9 alloys[J]. Journal of Materials Science & Technology,1998,14(4):323-326. |
APA | B. Varga,J. Takacs,A. Lovas,P. Kamasa,F. Zhou,&J. Vandlik.(1998).Comparison of the thermomagnetic and thermal effects during nanocrystallization of amorphous Fe76.5-xCu1NbxSi13.5B9 alloys.Journal of Materials Science & Technology,14(4),323-326. |
MLA | B. Varga,et al."Comparison of the thermomagnetic and thermal effects during nanocrystallization of amorphous Fe76.5-xCu1NbxSi13.5B9 alloys".Journal of Materials Science & Technology 14.4(1998):323-326. |
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