Microstructure and preparation of Ni, Al and Fe nanopowders | |
Q. Wei; Y. L. Lai; H. Yang; C. G. Li | |
1997 | |
发表期刊 | Transactions of Nonferrous Metals Society of China
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ISSN | 1003-6326 |
卷号 | 7期号:1页码:61-65 |
摘要 | By means of mechanical-physical solid state reaction methods (MPSSRM), 5 similar to 25 nm powders of iron, nickel, aluminium have been prepared. The powders exhibit few clusters of monocrystal and polycrystal, the eletronic structure of which were identified by X-ray diffraction and XPS. The experiments show that there is an oxide layer on the surfaces of Ni, Al, Fe nanopowders. DTA experiments show that the peak point temperature of primal temperature decreases with the decrease of the particle diameter, and tends to move in low temperature direction on the DTA curve of Fe nanopowder. The relationship between the particle diameter (d) of Fe nanopowder and surface energy (Delta H) can be given by Delta H(proportional to)d(-1/2). |
部门归属 | cent s univ technol,dept appl phys & heat engn,changsha 410083,peoples r china. acad sinica,int ctr mat phys,shenyang 110015,peoples r china. |
关键词 | Nanopowder Microstructure Electronic Structure Surface Energy |
URL | 查看原文 |
文献类型 | 期刊论文 |
条目标识符 | http://ir.imr.ac.cn/handle/321006/38140 |
专题 | 中国科学院金属研究所 |
推荐引用方式 GB/T 7714 | Q. Wei,Y. L. Lai,H. Yang,et al. Microstructure and preparation of Ni, Al and Fe nanopowders[J]. Transactions of Nonferrous Metals Society of China,1997,7(1):61-65. |
APA | Q. Wei,Y. L. Lai,H. Yang,&C. G. Li.(1997).Microstructure and preparation of Ni, Al and Fe nanopowders.Transactions of Nonferrous Metals Society of China,7(1),61-65. |
MLA | Q. Wei,et al."Microstructure and preparation of Ni, Al and Fe nanopowders".Transactions of Nonferrous Metals Society of China 7.1(1997):61-65. |
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