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HIGH-RESOLUTION ELECTRON-MICROSCOPY STUDIES OF THE MICROSTRUCTURE IN NANOCRYSTALLINE (FE0.99MO0.01)SI9B13 ALLOYS
D. H. Ping; D. X. Li; H. Q. Ye; X. D. Liu; Z. Q. Hu
1995
发表期刊Materials Science and Engineering a-Structural Materials Properties Microstructure and Processing
ISSN0921-5093
卷号194期号:2页码:211-217
摘要The crystallization process of an amorphous (Fe0.99Mo0.01)(78)Si9B13 alloy was examined by high resolution electron microscopy. Experimental results show that nanocrystalline alloys with average grain sizes in the range 30-50 nm are obtained after annealing at 560-620 degrees C for 1 h, and four phases - alpha-Fe(Si,Mo), (Fe, Mo)(3)B, (Fe,Mo)(23)B-6 and Fe2B - coexist in the sample. Most of the Fe2B crystals are found to nucleate at the interfaces between alpha-Fe(Si,Mo) grains and the residual amorphous phase at 620 degrees C. No disordered regions and nanovoids were detected at the grain boundaries. Defect structures in the nanocrystalline alloys are also discussed.
部门归属acad sinica,inst met res,atom imaging solids lab,shenyang 110015,peoples r china.;ping, dh (reprint author), acad sinica,inst met res,atom imaging solids lab,shenyang 110015,peoples r china
关键词Iron Molybdenum Silicon Boron Alloys Crystals Grain-structure Palladium Hrem
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文献类型期刊论文
条目标识符http://ir.imr.ac.cn/handle/321006/38648
专题中国科学院金属研究所
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GB/T 7714
D. H. Ping,D. X. Li,H. Q. Ye,et al. HIGH-RESOLUTION ELECTRON-MICROSCOPY STUDIES OF THE MICROSTRUCTURE IN NANOCRYSTALLINE (FE0.99MO0.01)SI9B13 ALLOYS[J]. Materials Science and Engineering a-Structural Materials Properties Microstructure and Processing,1995,194(2):211-217.
APA D. H. Ping,D. X. Li,H. Q. Ye,X. D. Liu,&Z. Q. Hu.(1995).HIGH-RESOLUTION ELECTRON-MICROSCOPY STUDIES OF THE MICROSTRUCTURE IN NANOCRYSTALLINE (FE0.99MO0.01)SI9B13 ALLOYS.Materials Science and Engineering a-Structural Materials Properties Microstructure and Processing,194(2),211-217.
MLA D. H. Ping,et al."HIGH-RESOLUTION ELECTRON-MICROSCOPY STUDIES OF THE MICROSTRUCTURE IN NANOCRYSTALLINE (FE0.99MO0.01)SI9B13 ALLOYS".Materials Science and Engineering a-Structural Materials Properties Microstructure and Processing 194.2(1995):211-217.
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