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Preparation of Fluoridated Hydroxyapatite Coatings on Titanium by Electrolytic Deposition and Its FTIR Characteristics
Y. Huang; X. F. Pang; G. Li; Y. J. Yan; S. G. Han; H. J. Zeng
2012
发表期刊Spectroscopy and Spectral Analysis
ISSN1000-0593
卷号32期号:7页码:1771-1774
摘要Fluoridated hydroxyapatite coatings (FHAP) were prepared on titanium substrate by electrochemical deposition technique containing Ca2+, PO43-, and F- ions. The deposition was all conducted at a constant current of 0.9 mA for 60 min at 60 degrees C. The as-prepared coatings were examined by scanning electron microscope (SEM), energy-dispersive Xray spectroscopy (EDS), Fourier transform infrared spectroscopy (FTIR) and Xray diffraction (XRD) tests. The results indicate that the FHAP cryatals take the morphology of nanoscale-rodlike cone rather than the micron-daisy petal, and the composite coating becomes more compact. The FTIR test indicates that the symmetry of stretching and bending vibration modes of hydroxyl changed, simulated body fluid immersion test proved that the FHAP coating had induced carbonate-apatite formation, indicating that the composite coating possesses excellent biocompatibility.
部门归属[huang yong; pang xiao-feng; li gun; yan ya-jing; han shu-guang; zeng hong-juan] univ elect sci & technol china, key lab neuroinformat, inst life sci & technol, minist educ, chengdu 610054, peoples r china. [pang xiao-feng] chinese acad sci, int ctr mat phys, shenyang 110015, peoples r china.;pang, xf (reprint author), univ elect sci & technol china, key lab neuroinformat, inst life sci & technol, minist educ, chengdu 610054, peoples r china.;hyuestc@126.com; pangxf2006@yahoo.com.cn
关键词Electrolytic Deposition Fluoridated Hydroxyapatite Coatings Fourier Transform Infrared Spectroscopy Alloy
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文献类型期刊论文
条目标识符http://ir.imr.ac.cn/handle/321006/60014
专题中国科学院金属研究所
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GB/T 7714
Y. Huang,X. F. Pang,G. Li,et al. Preparation of Fluoridated Hydroxyapatite Coatings on Titanium by Electrolytic Deposition and Its FTIR Characteristics[J]. Spectroscopy and Spectral Analysis,2012,32(7):1771-1774.
APA Y. Huang,X. F. Pang,G. Li,Y. J. Yan,S. G. Han,&H. J. Zeng.(2012).Preparation of Fluoridated Hydroxyapatite Coatings on Titanium by Electrolytic Deposition and Its FTIR Characteristics.Spectroscopy and Spectral Analysis,32(7),1771-1774.
MLA Y. Huang,et al."Preparation of Fluoridated Hydroxyapatite Coatings on Titanium by Electrolytic Deposition and Its FTIR Characteristics".Spectroscopy and Spectral Analysis 32.7(2012):1771-1774.
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