Synthesis and Characterization of Niobium-doped TiO2 Nanotube Arrays by Anodization of Ti-20Nb Alloys | |
Z. C. Xu; Q. Li; S. A. Gao; J. K. Shang | |
2012 | |
发表期刊 | Journal of Materials Science & Technology
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ISSN | 1005-0302 |
卷号 | 28期号:10页码:865-870 |
摘要 | Well crystallized niobium-doped TiO2 nanotube arrays (TiNbO-NT) were successfully synthesized via the anodization of titanium/niobium alloy sheets, followed with a heat treatment at 550 degrees C for 2 h. Morphology analysis results demonstrated that both the titanium/niobium alloy microstructure and the dissolution strength of electrolyte played major roles in the formation of nanotube structure. A single-phase microstructure was more favorable to the formation of uniform nanotube arrays, while modulating the dissolution strength of electrolyte was required to obtain nanotube arrays from the alloys with multi-phase microstructures. X-ray diffraction (XRD) and X-ray photoelectron (XPS) analysis results clearly demonstrated that niobium dopants (Nb5+) were successfully doped into TiO2 anatase lattice by substituting Ti4+ in this approach. |
部门归属 | [xu, zhengchao; li, qi; gao, shian; shang, jianku] chinese acad sci, mat ctr water purificat, shenyang natl lab mat sci, inst met res, shenyang 110016, peoples r china. [shang, jianku] univ illinois, dept mat sci & engn, urbana, il 61801 usa.;li, q (reprint author), chinese acad sci, mat ctr water purificat, shenyang natl lab mat sci, inst met res, shenyang 110016, peoples r china.;qili@imr.ac.cn |
关键词 | Tio2 Nanotube Arrays Anodization Doping Sensitized Solar-cells Photocatalytic Activity Anatase Tio2 Titanium-dioxide Mesoporous Tio2 Light Films Recombination Nanoparticles Powders |
URL | 查看原文 |
文献类型 | 期刊论文 |
条目标识符 | http://ir.imr.ac.cn/handle/321006/60376 |
专题 | 中国科学院金属研究所 |
推荐引用方式 GB/T 7714 | Z. C. Xu,Q. Li,S. A. Gao,et al. Synthesis and Characterization of Niobium-doped TiO2 Nanotube Arrays by Anodization of Ti-20Nb Alloys[J]. Journal of Materials Science & Technology,2012,28(10):865-870. |
APA | Z. C. Xu,Q. Li,S. A. Gao,&J. K. Shang.(2012).Synthesis and Characterization of Niobium-doped TiO2 Nanotube Arrays by Anodization of Ti-20Nb Alloys.Journal of Materials Science & Technology,28(10),865-870. |
MLA | Z. C. Xu,et al."Synthesis and Characterization of Niobium-doped TiO2 Nanotube Arrays by Anodization of Ti-20Nb Alloys".Journal of Materials Science & Technology 28.10(2012):865-870. |
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