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题名: One-pot synthesis of Ni/Ni3C/Ni3N nanocomposite: Structure, growth mechanism and magnetic properties
作者: Zhu, Yuan;  Zhang, Yajing;  Wang, Kangjun;  Li, Da;  Ding, Fu;  Meng, Dan;  Wang, Xiaolei;  Zhang, Zhidong
发表日期: 2017-11-1
摘要: A one-pot solvothermal synthesis of Ni/Ni3C/Ni3N nanocomposite, using hydrazine hydrate (N2H4) as reducing agent and tetraethylene glycol (TEG) as solvent, is reported. The contents of Ni3C and Ni3N decrease with increasing the amount of N2H4. The magnetic hysteresis loops at room temperature of the Ni/Ni3C/Ni3N display ferromagnetic characteristics. Saturation magnetization increases gradually with increasing Ni content of the Ni/Ni3C/Ni3N. Growth mechanism is discussed based on the characterization results of X-ray diffraction (XRD), scanning electron microscope (SEM), and X-ray photoelectron spectroscopy (XPS), thermogravimetric analysis (TG), nitrogen adsorption desorption, and elemental analysis. Furthermore, Ni3N was fabricated by such a solution chemistry method at low-temperature of 200 degrees C. (C) 2017 Elsevier Ltd. All rights reserved.
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Recommended Citation:
Zhu, Yuan,Zhang, Yajing,Wang, Kangjun,et al. One-pot Synthesis Of Ni/ni3c/ni3n Nanocomposite: Structure, Growth Mechanism And Magnetic Properties[J]. Pergamon-elsevier Science Ltd,2017,95:79-85.

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