One-pot synthesis of Ni/Ni3C/Ni3N nanocomposite: Structure, growth mechanism and magnetic properties

IMR OpenIR

	One-pot synthesis of Ni/Ni3C/Ni3N nanocomposite: Structure, growth mechanism and magnetic properties
	Zhu, Yuan; Zhang, Yajing; Wang, Kangjun; Li, Da; Ding, Fu; Meng, Dan; Wang, Xiaolei; Zhang, Zhidong; Zhang, YJ (reprint author), Shenyang Univ Chem Technol, Coll Chem Engn, Shenyang 110142, Liaoning, Peoples R China.; Li, D (reprint author), Chinese Acad Sci, Shenyang Natl Lab Mat Sci, Inst Met Res, Shenyang 110016, Liaoning, Peoples R China.
	2017-11-01
发表期刊	PERGAMON-ELSEVIER SCIENCE LTD
ISSN	0025-5408
卷号	95 页码:79-85
摘要	A one-pot solvothermal synthesis of Ni/Ni3C/Ni3N nanocomposite, using hydrazine hydrate (N2H4) as reducing agent and tetraethylene glycol (TEG) as solvent, is reported. The contents of Ni3C and Ni3N decrease with increasing the amount of N2H4. The magnetic hysteresis loops at room temperature of the Ni/Ni3C/Ni3N display ferromagnetic characteristics. Saturation magnetization increases gradually with increasing Ni content of the Ni/Ni3C/Ni3N. Growth mechanism is discussed based on the characterization results of X-ray diffraction (XRD), scanning electron microscope (SEM), and X-ray photoelectron spectroscopy (XPS), thermogravimetric analysis (TG), nitrogen adsorption desorption, and elemental analysis. Furthermore, Ni3N was fabricated by such a solution chemistry method at low-temperature of 200 degrees C. (C) 2017 Elsevier Ltd. All rights reserved.; A one-pot solvothermal synthesis of Ni/Ni3C/Ni3N nanocomposite, using hydrazine hydrate (N2H4) as reducing agent and tetraethylene glycol (TEG) as solvent, is reported. The contents of Ni3C and Ni3N decrease with increasing the amount of N2H4. The magnetic hysteresis loops at room temperature of the Ni/Ni3C/Ni3N display ferromagnetic characteristics. Saturation magnetization increases gradually with increasing Ni content of the Ni/Ni3C/Ni3N. Growth mechanism is discussed based on the characterization results of X-ray diffraction (XRD), scanning electron microscope (SEM), and X-ray photoelectron spectroscopy (XPS), thermogravimetric analysis (TG), nitrogen adsorption desorption, and elemental analysis. Furthermore, Ni3N was fabricated by such a solution chemistry method at low-temperature of 200 degrees C. (C) 2017 Elsevier Ltd. All rights reserved.
部门归属	[zhu, yuan ; zhang, yajing ; wang, kangjun ; ding, fu ; meng, dan] shenyang univ chem technol, coll chem engn, shenyang 110142, liaoning, peoples r china ; [li, da ; zhang, zhidong] chinese acad sci, shenyang natl lab mat sci, inst met res, shenyang 110016, liaoning, peoples r china ; [wang, xiaolei] shenyang univ technol, sch sci, shenyang 110870, liaoning, peoples r china
关键词	Ni3c Ni3n Solvothermal Method Magnetic Property
学科领域	Materials Science, Multidisciplinary
资助者	National Nature Science Foundation of China [51301114, 51371175, 61403263, 21201123, 21203125, 51601120]; SRF for ROCS, SEM [[2010]1174]; Natural Science Foundation of Liaoning Province [201602598, 2015020649]; LNET [LJQ2013044]
收录类别	SCI
语种	英语
WOS记录号	WOS:000412378500010
引用统计	被引频次：7[WOS] [WOS记录] [WOS相关记录]
文献类型	期刊论文
条目标识符	http://ir.imr.ac.cn/handle/321006/79019
专题	中国科学院金属研究所
通讯作者	Zhang, YJ (reprint author), Shenyang Univ Chem Technol, Coll Chem Engn, Shenyang 110142, Liaoning, Peoples R China.; Li, D (reprint author), Chinese Acad Sci, Shenyang Natl Lab Mat Sci, Inst Met Res, Shenyang 110016, Liaoning, Peoples R China.
推荐引用方式 GB/T 7714	Zhu, Yuan,Zhang, Yajing,Wang, Kangjun,et al. One-pot synthesis of Ni/Ni3C/Ni3N nanocomposite: Structure, growth mechanism and magnetic properties[J]. PERGAMON-ELSEVIER SCIENCE LTD,2017,95:79-85.
APA	Zhu, Yuan.,Zhang, Yajing.,Wang, Kangjun.,Li, Da.,Ding, Fu.,...&Li, D .(2017).One-pot synthesis of Ni/Ni3C/Ni3N nanocomposite: Structure, growth mechanism and magnetic properties.PERGAMON-ELSEVIER SCIENCE LTD,95,79-85.
MLA	Zhu, Yuan,et al."One-pot synthesis of Ni/Ni3C/Ni3N nanocomposite: Structure, growth mechanism and magnetic properties".PERGAMON-ELSEVIER SCIENCE LTD 95(2017):79-85.