Variation of nanoparticle fraction and compositions in two-stage double peaks aging precipitation of Al-Zn-Mg alloy | |
Wang, YL; Song, YY; Jiang, HC; Li, ZM; Zhang, D; Rong, LJ; Rong, LJ (reprint author), Chinese Acad Sci, Inst Met Res, CAS Key Lab Nucl Mat & Safety Assessment, Shenyang 110016, Peoples R China. | |
2018-04-27 | |
发表期刊 | NANOSCALE RESEARCH LETTERS
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ISSN | 1556-276X |
卷号 | 13页码:- |
摘要 | Atom probe tomography (APT) coupling high-resolution transmission electron microscopy (HRTEM) was used to analyze the fraction and compositions of different nanoparticles in two-stage double peaks aging process of Al-Zn -Mg alloy. Al content is found to be closely related to the size of nanoparticles and it can be greater than similar to 50.0 at. % in the nanoparticle with the equivalent radius under similar to 3.0 nm. Correspondingly, Al content of the nanoparticle, with the equivalent radius over similar to 5.0 nm, is measured under similar to 40.0 at. %. Evolution from Guinier-Preston (G.P.) zone to. phase is a growing process where Mg and Zn atoms enter the nanoparticle, therefore rejecting Al atoms. G.P. zones can take up a number fraction of similar to 85.0 and similar to 22.7% of nanoparticles in the first and second peak-aged samples, respectively, and even in the over-aged (T73) sample, they can still be found. As aging time increases, fraction of eta' phases monotonically rises to the peak value (similar to 54.5%) in the second peak-aged state and then drops, which is significant for the second hardness peak and directly proves their function as the transitional medium. In T73 state, similar to 63.3% nanoparticles compose of. phases, which were measured to still contain similar to 10.2 to similar to 36.4 at. % Al atoms.; Atom probe tomography (APT) coupling high-resolution transmission electron microscopy (HRTEM) was used to analyze the fraction and compositions of different nanoparticles in two-stage double peaks aging process of Al-Zn -Mg alloy. Al content is found to be closely related to the size of nanoparticles and it can be greater than similar to 50.0 at. % in the nanoparticle with the equivalent radius under similar to 3.0 nm. Correspondingly, Al content of the nanoparticle, with the equivalent radius over similar to 5.0 nm, is measured under similar to 40.0 at. %. Evolution from Guinier-Preston (G.P.) zone to. phase is a growing process where Mg and Zn atoms enter the nanoparticle, therefore rejecting Al atoms. G.P. zones can take up a number fraction of similar to 85.0 and similar to 22.7% of nanoparticles in the first and second peak-aged samples, respectively, and even in the over-aged (T73) sample, they can still be found. As aging time increases, fraction of eta' phases monotonically rises to the peak value (similar to 54.5%) in the second peak-aged state and then drops, which is significant for the second hardness peak and directly proves their function as the transitional medium. In T73 state, similar to 63.3% nanoparticles compose of. phases, which were measured to still contain similar to 10.2 to similar to 36.4 at. % Al atoms. |
部门归属 | [wang, y. l. ; song, y. y. ; jiang, h. c. ; li, z. m. ; zhang, d. ; rong, l. j.] chinese acad sci, inst met res, cas key lab nucl mat & safety assessment, shenyang 110016, peoples r china ; [wang, y. l. ; zhang, d.] univ sci & technol china, sch mat sci & engn, hefei 230026, peoples r china |
关键词 | Atom-probe Analysis Aluminum-alloys Gp-zones Resistance Corrosion Rra |
学科领域 | Nanoscience & Nanotechnology ; Materials Science, Multidisciplinary ; Physics, Applied |
资助者 | National Key R&D Program of China [2016YFB1200504]; Strategic Priority Program of the Chinese Academy of Sciences [XDB22000000] |
收录类别 | SCI |
语种 | 英语 |
WOS记录号 | WOS:000431084400005 |
引用统计 | |
文献类型 | 期刊论文 |
条目标识符 | http://ir.imr.ac.cn/handle/321006/79354 |
专题 | 中国科学院金属研究所 |
通讯作者 | Jiang, HC; Rong, LJ (reprint author), Chinese Acad Sci, Inst Met Res, CAS Key Lab Nucl Mat & Safety Assessment, Shenyang 110016, Peoples R China. |
推荐引用方式 GB/T 7714 | Wang, YL,Song, YY,Jiang, HC,et al. Variation of nanoparticle fraction and compositions in two-stage double peaks aging precipitation of Al-Zn-Mg alloy[J]. NANOSCALE RESEARCH LETTERS,2018,13:-. |
APA | Wang, YL.,Song, YY.,Jiang, HC.,Li, ZM.,Zhang, D.,...&Rong, LJ .(2018).Variation of nanoparticle fraction and compositions in two-stage double peaks aging precipitation of Al-Zn-Mg alloy.NANOSCALE RESEARCH LETTERS,13,-. |
MLA | Wang, YL,et al."Variation of nanoparticle fraction and compositions in two-stage double peaks aging precipitation of Al-Zn-Mg alloy".NANOSCALE RESEARCH LETTERS 13(2018):-. |
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