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EFFECTS OF FORGING AND HEAT TREATMENTS ON STRESS CORROSION BEHAVIOR OF 316LN STAINLESS STEEL IN HIGH TEMPERATURE CAUSTIC SOLUTION
Guo Yueling1,2; Han En-Hou1,2; Wang Jianqiu2
通讯作者Han En-Hou(ehhan@imr.ac.cn)
2015-06-11
发表期刊ACTA METALLURGICA SINICA
ISSN0412-1961
卷号51期号:6页码:659-667
摘要The reactor coolant piping in the third generation nuclear power plants of AP1000 is manufactured by integrally forging. Therefore, it is of vital importance to investigate the effects of forging and heat treatments on the stress corrosion cracking (SCC) resistance of 316LN stainless steel (316LNSS), which is the candidate material for the reactor coolant piping in AP1000 nuclear power plants. In this work, electron back scattering diffraction (EBSD) and microhardness measurements (HV) were used to characterize the microstructure and residual strain of the as-received 316LNSS, the forged and solution anneal treated 316LNSS and the forged and stress relief treated 316LNSS, respectively. The average grain size of the as-received 316LNSS was the largest, and the forged 316LNSS followed by solution anneal treatment and stress relief treatment showed no obvious differences on grain size. The as-received 316LNSS exhibited the highest residual strain followed by the forged and stress relief treated 316LNSS and then solution anneal treated 316LNSS. Besides, the residual strain in the as-received 316LNSS concentrated on grain boundaries, while the residual strain in the forged and stress relief treated 316LNSS was characterized by a band-like distribution. The U-bend specimens were utilized to investigate the SCC behavior of the 3 kinds of 316LNSS specimens in high temperature caustic solution. After SCC experiments, the crack morphologies of the 3 kinds of 316LNSS specimens were examined by SEM. Then the macro and micro fracture morphologies were examined by OM and SEM, respectively. Grain morphology, residual strain and grain boundary character distribution near the SCC crack tip of the forged and stress relief treated 316LNSS were investigated using EBSD. The results showed that the forged and solution anneal treated 316LNSS exhibited the lowest SCC sensibility, while the as-received the highest, with the most cracks and the highest growth rate. The as-received and the forged and solution anneal treated 316LNSS showed obvious intergranular cracking, while the forged and stress relief treated 316LNSS showed a mixed cracking mode. The larger average grain size and higher residual Strain, especially concentrating on the grain boundaries, were considered to be responsible for the highest SCC sensibility of the as-received 316LNSS. Compared with the forged and stress relief treated 316LNSS, the higher content of coincidence site lattice boundary (CSLB) and lower residual strain contributed to the lower SCC sensibility of forged and solution anneal treated 316LNSS. The stress relief treatment failed to eliminate the band-like microstructure effectively, which disadvantaged the SCC resistance.
关键词stainless steel nuclear material stress corrosion cracking high temperature caustic solution fractography
收录类别SCI
语种英语
WOS研究方向Metallurgy & Metallurgical Engineering
WOS类目Metallurgy & Metallurgical Engineering
WOS记录号WOS:000356639800003
出版者SCIENCE PRESS
引用统计
文献类型期刊论文
条目标识符http://ir.imr.ac.cn/handle/321006/81121
专题中国科学院金属研究所
通讯作者Han En-Hou
作者单位1.Univ Sci & Technol Beijing, Natl Ctr Mat Serv Safety, Beijing 100083, Peoples R China
2.Chinese Acad Sci, Inst Met Res, Key Lab Nucl Mat & Safety Assessment, Shenyang 110016, Peoples R China
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GB/T 7714
Guo Yueling,Han En-Hou,Wang Jianqiu. EFFECTS OF FORGING AND HEAT TREATMENTS ON STRESS CORROSION BEHAVIOR OF 316LN STAINLESS STEEL IN HIGH TEMPERATURE CAUSTIC SOLUTION[J]. ACTA METALLURGICA SINICA,2015,51(6):659-667.
APA Guo Yueling,Han En-Hou,&Wang Jianqiu.(2015).EFFECTS OF FORGING AND HEAT TREATMENTS ON STRESS CORROSION BEHAVIOR OF 316LN STAINLESS STEEL IN HIGH TEMPERATURE CAUSTIC SOLUTION.ACTA METALLURGICA SINICA,51(6),659-667.
MLA Guo Yueling,et al."EFFECTS OF FORGING AND HEAT TREATMENTS ON STRESS CORROSION BEHAVIOR OF 316LN STAINLESS STEEL IN HIGH TEMPERATURE CAUSTIC SOLUTION".ACTA METALLURGICA SINICA 51.6(2015):659-667.
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