Technical Note: A High-Temperature, High-Pressure Window for In Situ Optical Observation and Raman Detection

doi:10.5006/1617

IMR OpenIR

	Technical Note: A High-Temperature, High-Pressure Window for In Situ Optical Observation and Raman Detection
	Kuang, Wenjun 1,2,3; Wu, Xinqiang 1; Wang, Xiang 1; Han, En-Hou 1
通讯作者	Wu, Xinqiang(xqwu@imr.ac.cn)
	2015-06-01
发表期刊	CORROSION
ISSN	0010-9312
卷号	71 期号:6 页码:687-691
摘要	A window was developed on a high-temperature, high-pressure refreshed autoclave to perform in situ tests. High-purity single crystal sapphire was used as window material to withstand the harsh environment and minimize the production of fluorescence. The cone-shaped internal structure enables a large light flux necessary for the in situ optical observation. Through this window, in situ optical observation and Raman tests were successfully performed in high-temperature, high-pressure water using a long-distance microscope and a custom-made Raman system. The formation of spinel oxide on 304 stainless steel in oxygenated water containing a high concentration of Ni cations was verified by in situ Raman tests.
关键词	cracking oxidation Raman spectroscopy
资助者	Science and Technology Foundation of China ; Special Funds for the Major State Basic Research Projects ; Innovation Fund of Institute of Metal Research, Chinese Academy of Sciences
DOI	10.5006/1617
收录类别	SCI
语种	英语
资助项目	Science and Technology Foundation of China[51371174] ; Special Funds for the Major State Basic Research Projects[2011CB610505] ; Innovation Fund of Institute of Metal Research, Chinese Academy of Sciences
WOS研究方向	Materials Science ; Metallurgy & Metallurgical Engineering
WOS类目	Materials Science, Multidisciplinary ; Metallurgy & Metallurgical Engineering
WOS记录号	WOS:000355559700001
出版者	NATL ASSOC CORROSION ENG
引用统计
文献类型	期刊论文
条目标识符	http://ir.imr.ac.cn/handle/321006/81152
通讯作者	Wu, Xinqiang
作者单位	1.Chinese Acad Sci, Inst Met Res, Key Lab Nucl Mat & Safety Assessment, Liaoning Key Lab Safety & Assessment Tech Nucl Ma, Shenyang 110016, Peoples R China 2.Univ Michigan, Ann Arbor, MI 48109 USA 3.Chinese Acad Sci, Inst Met Res, Shenyang 110016, Peoples R China
推荐引用方式 GB/T 7714	Kuang, Wenjun,Wu, Xinqiang,Wang, Xiang,et al. Technical Note: A High-Temperature, High-Pressure Window for In Situ Optical Observation and Raman Detection[J]. CORROSION,2015,71(6):687-691.
APA	Kuang, Wenjun,Wu, Xinqiang,Wang, Xiang,&Han, En-Hou.(2015).Technical Note: A High-Temperature, High-Pressure Window for In Situ Optical Observation and Raman Detection.CORROSION,71(6),687-691.
MLA	Kuang, Wenjun,et al."Technical Note: A High-Temperature, High-Pressure Window for In Situ Optical Observation and Raman Detection".CORROSION 71.6(2015):687-691.