Synthesis and size control of NiO nanoparticles by water-in-oil microemulsion

doi:10.1016/j.powtec.2004.09.024

IMR OpenIR

	Synthesis and size control of NiO nanoparticles by water-in-oil microemulsion
	Han, DY ; Yang, HY ; Shen, CB ; Zhou, X ; Wang, FH
通讯作者	Han, DY(dyhan@imr.ac.cn)
	2004-10-11
发表期刊	POWDER TECHNOLOGY
ISSN	0032-5910
卷号	147 期号:1-3 页码:113-116
摘要	Nanoparticles of NiO were successfully prepared by Triton X-100/n-hextnol/cyclohexane/water W/O microemulsion system. Basic synthesis parameters were determined. The result of TG-DTA analysis of the precursor products showed that the proper calcination temperature was 450 degreesC. The nanoparticles were characterized by X-ray diffractometer (XRD), transmission electron microscopy (TEM) and UV-VIS spectra. The results showed that the nanoparticle was exactly NiO with cubic rock salt structure and the size of nanoparticles was strongly affected by the ratio of water to surfactant (R) and also the calcined temperature. With the R value increased, the particles size became larger; with the calcined temperature increased, the particles size also became larger. (C) 2004 Elsevier B.V. All rights reserved.
关键词	microemulsion NiO nanoparticles synthesis
DOI	10.1016/j.powtec.2004.09.024
收录类别	SCI
语种	英语
WOS研究方向	Engineering
WOS类目	Engineering, Chemical
WOS记录号	WOS:000225808900011
出版者	ELSEVIER SCIENCE SA
引用统计
文献类型	期刊论文
条目标识符	http://ir.imr.ac.cn/handle/321006/81608
通讯作者	Han, DY
作者单位	1.Chinese Acad Sci, Inst Met Res, State Key Lab Corros & Protect, Shenyang 110016, Peoples R China 2.Dalian Inst Railway Technol, Dept Mat Sci & Engn, Dalian 116028, Peoples R China
推荐引用方式 GB/T 7714	Han, DY,Yang, HY,Shen, CB,et al. Synthesis and size control of NiO nanoparticles by water-in-oil microemulsion[J]. POWDER TECHNOLOGY,2004,147(1-3):113-116.
APA	Han, DY,Yang, HY,Shen, CB,Zhou, X,&Wang, FH.(2004).Synthesis and size control of NiO nanoparticles by water-in-oil microemulsion.POWDER TECHNOLOGY,147(1-3),113-116.
MLA	Han, DY,et al."Synthesis and size control of NiO nanoparticles by water-in-oil microemulsion".POWDER TECHNOLOGY 147.1-3(2004):113-116.