| Preparation of size controllable MgO nanoparticles via reverse microemulsion method | |
| Han, DY; Yang, HY; Shen, CB | |
| Corresponding Author | Han, DY(dyhan@imr.ac.cn) |
| 2005 | |
| Source Publication | PRICM 5: THE FIFTH PACIFIC RIM INTERNATIONAL CONFERENCE ON ADVANCED MATERIALS AND PROCESSING, PTS 1-5
 |
| ISSN | 0255-5476 |
| Volume | 475-479Pages:3543-3546 |
| Abstract | Nanoparticles of MgO were successfully prepared in Triton X-100/n-hextnol/cyclohexane/water W/O microemulsion system. Basic preparation conditions were determined. TG-DTA showed that the proper calcination temperature was 450 degrees C. The nanoparticles were characterized by XRD and IR measurements in order to determine the crystal phase and component of the products. The morphological feature of the nanoparticles has been investigated by TEM. The result of XRD pattern demonstrated that the particles were exactly indexed to a cubic rock salt structure of MgO. There are no organic or inorganic impurities appeared after 450 degrees C calcination. The result of TEM showed that the MgO nanoparticles were spherical and uniform. The UV-visible spectra demonstrated the phenomenon of absorption blue shift, which is the evidence of quantum confinement effect, with the decrease of water/surfactant(R) value. Average size of the nanoparticles increased with increasing R value. |
| Keyword | preparation MgO nanoparticles microemulsion |
| Indexed By | SCI |
| Language | 英语 |
| WOS Research Area | Materials Science ; Metallurgy & Metallurgical Engineering |
| WOS Subject | Materials Science, Multidisciplinary ; Metallurgy & Metallurgical Engineering |
| WOS ID | WOS:000227494704046 |
| Publisher | TRANS TECH PUBLICATIONS LTD |
| Citation statistics | |
| Document Type | 期刊论文 |
| Identifier | http://ir.imr.ac.cn/handle/321006/83020 |
| Corresponding Author | Han, DY |
| Affiliation | 1.Chinese Acad Sci, Met Res Inst, State Key Lab Corros & Protect, Shenyang 110016, Peoples R China 2.Dalian Inst Railway Technol, Dept Mat Sci & Engn, Dalian 116028, Peoples R China |
| Recommended Citation GB/T 7714 | Han, DY,Yang, HY,Shen, CB. Preparation of size controllable MgO nanoparticles via reverse microemulsion method[J]. PRICM 5: THE FIFTH PACIFIC RIM INTERNATIONAL CONFERENCE ON ADVANCED MATERIALS AND PROCESSING, PTS 1-5,2005,475-479:3543-3546. |
| APA | Han, DY,Yang, HY,&Shen, CB.(2005).Preparation of size controllable MgO nanoparticles via reverse microemulsion method.PRICM 5: THE FIFTH PACIFIC RIM INTERNATIONAL CONFERENCE ON ADVANCED MATERIALS AND PROCESSING, PTS 1-5,475-479,3543-3546. |
| MLA | Han, DY,et al."Preparation of size controllable MgO nanoparticles via reverse microemulsion method".PRICM 5: THE FIFTH PACIFIC RIM INTERNATIONAL CONFERENCE ON ADVANCED MATERIALS AND PROCESSING, PTS 1-5 475-479(2005):3543-3546. |
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