In-situ reaction synthesis and decomposition of Ta2AlC | |
Hu, Chunfeng1,2; Zhang, Jie1,2; Bao, Yiwang1; Wang, Jingyang1; Li, Meishuan1; Zhou, Yanchun1 | |
通讯作者 | Zhou, Yanchun(yczhou@imr.ac.cn) |
2008 | |
发表期刊 | INTERNATIONAL JOURNAL OF MATERIALS RESEARCH
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ISSN | 1862-5282 |
卷号 | 99期号:1页码:8-13 |
摘要 | Dense bulk Ta2AlC ceramic was fabricated by in-situ reaction/hot pressing of Ta, Al and C powders. The reaction path and effects of initial composition on the purity were investigated. It was found that Ta2AlC formed through the reactions between AlTa2 and graphite, or between Ta5Al3C, TaC and graphite at 1500-1550 degrees C. By modifying the molar ratio of the initial Ta, Al, and C powders, single-phase Ta2AlC was prepared at 1550 degrees C under an Ar atmosphere with an optimized composition of Ta: Al: C = 2: 1.2: 0.9. The lattice parameter and a new set of X-ray diffraction data of Ta2AlC were obtained. In addition, Ta2AlC was reported unstable above 1600 degrees C and decomposed to Ta4AlC3, and then to TaCx. |
关键词 | Ta2AlC synthesis decomposition |
DOI | 10.3139/146.101598 |
收录类别 | SCI |
语种 | 英语 |
WOS研究方向 | Metallurgy & Metallurgical Engineering |
WOS类目 | Metallurgy & Metallurgical Engineering |
WOS记录号 | WOS:000252804500002 |
出版者 | CARL HANSER VERLAG |
引用统计 | |
文献类型 | 期刊论文 |
条目标识符 | http://ir.imr.ac.cn/handle/321006/94895 |
专题 | 中国科学院金属研究所 |
通讯作者 | Zhou, Yanchun |
作者单位 | 1.Chinese Acad Sci, Inst Met Res, Shenyang Natl Lab Mat Sci, Shenyang 110016, Peoples R China 2.Chinese Acad Sci, Grad Sch, Beijing, Peoples R China |
推荐引用方式 GB/T 7714 | Hu, Chunfeng,Zhang, Jie,Bao, Yiwang,et al. In-situ reaction synthesis and decomposition of Ta2AlC[J]. INTERNATIONAL JOURNAL OF MATERIALS RESEARCH,2008,99(1):8-13. |
APA | Hu, Chunfeng,Zhang, Jie,Bao, Yiwang,Wang, Jingyang,Li, Meishuan,&Zhou, Yanchun.(2008).In-situ reaction synthesis and decomposition of Ta2AlC.INTERNATIONAL JOURNAL OF MATERIALS RESEARCH,99(1),8-13. |
MLA | Hu, Chunfeng,et al."In-situ reaction synthesis and decomposition of Ta2AlC".INTERNATIONAL JOURNAL OF MATERIALS RESEARCH 99.1(2008):8-13. |
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