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Effect of Process Parameter on Properties of (Y,Gd)(2)O-3:Eu3+ Nanopowders Prepared by Co-Precipitation Method
Guo Yi-Fen1,2; Ma Wei-Min1; Wen Lei3; Shen Shi-Fei1; Wang Hua-Dong1; Yin Kai1
通讯作者Ma Wei-Min(maweimin56@163.com)
2009-05-01
发表期刊CHINESE JOURNAL OF INORGANIC CHEMISTRY
ISSN1001-4861
卷号25期号:5页码:880-885
摘要(Y,Gd)(2)O-3:Eu3+ nano-powders were prepared by forward-titration co-precipitation method and using ammonia as the precipitator. XRD, SEM and the fluorophotometer were used to analyze the morphology and characteristics of the powders. The results show that the near-spherical nano-powders with good dispersibility and fine particle size (30 similar to 60 nm) were obtained under the conditions of initial concentration of resolution, 0.15 mol . L-1, system temperature, 0 degrees C, titration rate, 2 mL . min(-1), stationary, 12 h and adding 3% (NH4)(2)SO4 (mass fraction). When adding 3% (NH4)(2)SO4, the nano-powders' Luminescent has unproved and the emission intensity of D-5(0)-> F-7(2) transition reaches the maximum.
关键词co-precipitation method process parameter synthesis and characterzation optical spectrum characteristic
收录类别SCI
语种英语
WOS研究方向Chemistry
WOS类目Chemistry, Inorganic & Nuclear
WOS记录号WOS:000266252500022
出版者CHINESE CHEMICAL SOC
引用统计
被引频次:3[WOS]   [WOS记录]     [WOS相关记录]
文献类型期刊论文
条目标识符http://ir.imr.ac.cn/handle/321006/97464
专题中国科学院金属研究所
通讯作者Ma Wei-Min
作者单位1.Shenyang Univ Chem Technol, Sch Mat Sci & Engn, Shenyang 110142, Peoples R China
2.Shenyang Univ, Coll Mech Engn, Shenyang 110044, Peoples R China
3.Chinese Acad Sci, Inst Met Res, Shenyang Natl Lab Mat Sci, Shenyang 110016, Peoples R China
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GB/T 7714
Guo Yi-Fen,Ma Wei-Min,Wen Lei,et al. Effect of Process Parameter on Properties of (Y,Gd)(2)O-3:Eu3+ Nanopowders Prepared by Co-Precipitation Method[J]. CHINESE JOURNAL OF INORGANIC CHEMISTRY,2009,25(5):880-885.
APA Guo Yi-Fen,Ma Wei-Min,Wen Lei,Shen Shi-Fei,Wang Hua-Dong,&Yin Kai.(2009).Effect of Process Parameter on Properties of (Y,Gd)(2)O-3:Eu3+ Nanopowders Prepared by Co-Precipitation Method.CHINESE JOURNAL OF INORGANIC CHEMISTRY,25(5),880-885.
MLA Guo Yi-Fen,et al."Effect of Process Parameter on Properties of (Y,Gd)(2)O-3:Eu3+ Nanopowders Prepared by Co-Precipitation Method".CHINESE JOURNAL OF INORGANIC CHEMISTRY 25.5(2009):880-885.
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