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Synthesis of Ti3SiC2 by high energy ball milling and reactive sintering from Ti, Si, and C elements
Meng, Fanling1,2,3; Chaffron, Laurent1; Zhou, Yanchun3
Corresponding AuthorChaffron, Laurent(laurent.chaffron@cea.fr)
2009-04-30
Source PublicationJOURNAL OF NUCLEAR MATERIALS
ISSN0022-3115
Volume386-88Pages:647-649
AbstractWe present an original method of preparation of nanostructured Ti3SiC2 compound based on high energy ball milling and reactive sintering techniques. Starting materials are Ti, Si, and C elements. X-ray diffraction and secondary electron microscopy are used to identify the formed phases and to analyze the obtained microstructures. Lower milling intensity and shorter milling time are found as the best milling conditions in order to get an intimate mixture of the three elements without formation of detectable secondary phases. The optimized sintering temperature is equal to 1350 degrees C. A method used for minimizing the oxygen content in the final compound is presented. (c) 2008 Elsevier B.V. All rights reserved.
DOI10.1016/j.jnucmat.2008.12.321
Indexed BySCI
Language英语
WOS Research AreaMaterials Science ; Nuclear Science & Technology ; Mining & Mineral Processing
WOS SubjectMaterials Science, Multidisciplinary ; Nuclear Science & Technology ; Mining & Mineral Processing
WOS IDWOS:000266386900161
PublisherELSEVIER SCIENCE BV
Citation statistics
Cited Times:13[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.imr.ac.cn/handle/321006/99108
Collection中国科学院金属研究所
Corresponding AuthorChaffron, Laurent
Affiliation1.CEA Saclay, DENDANS, DMN, SRMP,SRMA,LTMEX, F-91191 Gif Sur Yvette, France
2.Chinese Acad Sci, Grad Sch, Inst Met Res, Shenyang Natl Lab Mat Sci, Beijing 100039, Peoples R China
3.Chinese Acad Sci, Inst Met Res, Shenyang Natl Lab Mat Sci, Shenyang 110016, Peoples R China
Recommended Citation
GB/T 7714
Meng, Fanling,Chaffron, Laurent,Zhou, Yanchun. Synthesis of Ti3SiC2 by high energy ball milling and reactive sintering from Ti, Si, and C elements[J]. JOURNAL OF NUCLEAR MATERIALS,2009,386-88:647-649.
APA Meng, Fanling,Chaffron, Laurent,&Zhou, Yanchun.(2009).Synthesis of Ti3SiC2 by high energy ball milling and reactive sintering from Ti, Si, and C elements.JOURNAL OF NUCLEAR MATERIALS,386-88,647-649.
MLA Meng, Fanling,et al."Synthesis of Ti3SiC2 by high energy ball milling and reactive sintering from Ti, Si, and C elements".JOURNAL OF NUCLEAR MATERIALS 386-88(2009):647-649.
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