| One-pot synthesis of Ni/Ni3C/Ni3N nanocomposite: Structure, growth mechanism and magnetic properties | |
| Zhu, Yuan; Zhang, Yajing; Wang, Kangjun; Li, Da; Ding, Fu; Meng, Dan; Wang, Xiaolei; Zhang, Zhidong; Zhang, YJ (reprint author), Shenyang Univ Chem Technol, Coll Chem Engn, Shenyang 110142, Liaoning, Peoples R China.; Li, D (reprint author), Chinese Acad Sci, Shenyang Natl Lab Mat Sci, Inst Met Res, Shenyang 110016, Liaoning, Peoples R China. | |
| 2017-11-01 | |
| Source Publication | PERGAMON-ELSEVIER SCIENCE LTD
 |
| ISSN | 0025-5408 |
| Volume | 95Pages:79-85 |
| Abstract | A one-pot solvothermal synthesis of Ni/Ni3C/Ni3N nanocomposite, using hydrazine hydrate (N2H4) as reducing agent and tetraethylene glycol (TEG) as solvent, is reported. The contents of Ni3C and Ni3N decrease with increasing the amount of N2H4. The magnetic hysteresis loops at room temperature of the Ni/Ni3C/Ni3N display ferromagnetic characteristics. Saturation magnetization increases gradually with increasing Ni content of the Ni/Ni3C/Ni3N. Growth mechanism is discussed based on the characterization results of X-ray diffraction (XRD), scanning electron microscope (SEM), and X-ray photoelectron spectroscopy (XPS), thermogravimetric analysis (TG), nitrogen adsorption desorption, and elemental analysis. Furthermore, Ni3N was fabricated by such a solution chemistry method at low-temperature of 200 degrees C. (C) 2017 Elsevier Ltd. All rights reserved.; A one-pot solvothermal synthesis of Ni/Ni3C/Ni3N nanocomposite, using hydrazine hydrate (N2H4) as reducing agent and tetraethylene glycol (TEG) as solvent, is reported. The contents of Ni3C and Ni3N decrease with increasing the amount of N2H4. The magnetic hysteresis loops at room temperature of the Ni/Ni3C/Ni3N display ferromagnetic characteristics. Saturation magnetization increases gradually with increasing Ni content of the Ni/Ni3C/Ni3N. Growth mechanism is discussed based on the characterization results of X-ray diffraction (XRD), scanning electron microscope (SEM), and X-ray photoelectron spectroscopy (XPS), thermogravimetric analysis (TG), nitrogen adsorption desorption, and elemental analysis. Furthermore, Ni3N was fabricated by such a solution chemistry method at low-temperature of 200 degrees C. (C) 2017 Elsevier Ltd. All rights reserved. |
| description.department | [zhu, yuan ; zhang, yajing ; wang, kangjun ; ding, fu ; meng, dan] shenyang univ chem technol, coll chem engn, shenyang 110142, liaoning, peoples r china ; [li, da ; zhang, zhidong] chinese acad sci, shenyang natl lab mat sci, inst met res, shenyang 110016, liaoning, peoples r china ; [wang, xiaolei] shenyang univ technol, sch sci, shenyang 110870, liaoning, peoples r china |
| Keyword | Ni3c Ni3n Solvothermal Method Magnetic Property |
| Subject Area | Materials Science, Multidisciplinary |
| Funding Organization | National Nature Science Foundation of China [51301114, 51371175, 61403263, 21201123, 21203125, 51601120]; SRF for ROCS, SEM [[2010]1174]; Natural Science Foundation of Liaoning Province [201602598, 2015020649]; LNET [LJQ2013044] |
| Indexed By | SCI |
| Language | 英语 |
| WOS ID | WOS:000412378500010 |
| Citation statistics | |
| Document Type | 期刊论文 |
| Identifier | http://ir.imr.ac.cn/handle/321006/79019 |
| Collection | 中国科学院金属研究所 |
| Corresponding Author | Zhang, YJ (reprint author), Shenyang Univ Chem Technol, Coll Chem Engn, Shenyang 110142, Liaoning, Peoples R China.; Li, D (reprint author), Chinese Acad Sci, Shenyang Natl Lab Mat Sci, Inst Met Res, Shenyang 110016, Liaoning, Peoples R China. |
| Recommended Citation GB/T 7714 | Zhu, Yuan,Zhang, Yajing,Wang, Kangjun,et al. One-pot synthesis of Ni/Ni3C/Ni3N nanocomposite: Structure, growth mechanism and magnetic properties[J]. PERGAMON-ELSEVIER SCIENCE LTD,2017,95:79-85. |
| APA | Zhu, Yuan.,Zhang, Yajing.,Wang, Kangjun.,Li, Da.,Ding, Fu.,...&Li, D .(2017).One-pot synthesis of Ni/Ni3C/Ni3N nanocomposite: Structure, growth mechanism and magnetic properties.PERGAMON-ELSEVIER SCIENCE LTD,95,79-85. |
| MLA | Zhu, Yuan,et al."One-pot synthesis of Ni/Ni3C/Ni3N nanocomposite: Structure, growth mechanism and magnetic properties".PERGAMON-ELSEVIER SCIENCE LTD 95(2017):79-85. |
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