A simple method for the synthesis of nanosized Ti3AlC2 powder in NaCl-KCl molten salt

doi:10.1080/21663831.2019.1613695

IMR OpenIR

	A simple method for the synthesis of nanosized Ti3AlC2 powder in NaCl-KCl molten salt
	Yang, Ling Xu 1,2; Wang, Ying 1,2; Zhang, Hai Liang 1,2; Liu, Hui Jun 1; Zeng, Chao Liu 1
通讯作者	Liu, Hui Jun(liuhj@imr.ac.cn)
	2019
发表期刊	MATERIALS RESEARCH LETTERS
ISSN	2166-3831
卷号	7 期号:9 页码:361-367
摘要	Herein we report, a simple novel method to synthesize nanosized Ti3AlC2 powder from Ti, Al, and C powders in NaCl-KCl molten salt. It is more conducive to the formation of Ti3AlC2 at higher salt/precursor materials ratio and particle size of Ti3AlC2 powder dramatically decreases with increasing mass ratio of the salt to precursor materials. Fine-grained Ti3AlC2 powder is successfully synthesized at 950 degrees C for 5 h or at 1000 degrees C for 2 h with a salt/precursor materials ratio of 10:1. Ti3C2 MXene is also prepared by etching fine-grained Ti3AlC2 precursor in HF solution at 60 degrees C for 2 h. [GRAPHICS]
关键词	Ternary carbide Ti3AlC2 nanosized powder molten salt microstructure
资助者	National Natural Science Foundation of China
DOI	10.1080/21663831.2019.1613695
收录类别	SCI
语种	英语
资助项目	National Natural Science Foundation of China[51501205]
WOS研究方向	Materials Science
WOS类目	Materials Science, Multidisciplinary
WOS记录号	WOS:000471551600003
出版者	TAYLOR & FRANCIS INC
引用统计	被引频次：31[WOS] [WOS记录] [WOS相关记录]
文献类型	期刊论文
条目标识符	http://ir.imr.ac.cn/handle/321006/133975
专题	中国科学院金属研究所
通讯作者	Liu, Hui Jun
作者单位	1.Chinese Acad Sci, Inst Met Res, Lab Corros & Protect, Shenyang 110016, Liaoning, Peoples R China 2.Univ Sci & Technol China, Sch Mat Sci & Engn, Hefei, Anhui, Peoples R China
推荐引用方式 GB/T 7714	Yang, Ling Xu,Wang, Ying,Zhang, Hai Liang,et al. A simple method for the synthesis of nanosized Ti3AlC2 powder in NaCl-KCl molten salt[J]. MATERIALS RESEARCH LETTERS,2019,7(9):361-367.
APA	Yang, Ling Xu,Wang, Ying,Zhang, Hai Liang,Liu, Hui Jun,&Zeng, Chao Liu.(2019).A simple method for the synthesis of nanosized Ti3AlC2 powder in NaCl-KCl molten salt.MATERIALS RESEARCH LETTERS,7(9),361-367.
MLA	Yang, Ling Xu,et al."A simple method for the synthesis of nanosized Ti3AlC2 powder in NaCl-KCl molten salt".MATERIALS RESEARCH LETTERS 7.9(2019):361-367.