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Optimization of mixed silanes agent solution and curing process for composite gamma-glycidoxypropyl trimethoxysilane (gamma-GPS)/bis-1.2-(triethoxysilyl)ethane (BTSE) silane film on Q235 steel surfaceOptimierung von vermengten Silanlosungen und Aushartung fur gamma-glycidoxypropyl trimethoxysilan (gamma-GPS)/bis-1,2-(triethoxysilyl)athan (BTSE)-Komposit-Silanschicht auf einer Stahloberflache (Q 235)
Sun, Z. D.1,2,3; Yang, Y. N.1; Li, Q. K.3; Liu, J. G.3; Xu, Q.1,4; Yan, C. W.3
Corresponding AuthorSun, Z. D.(sunzd@sie.edu.cn)
2020-04-01
Source PublicationMATERIALWISSENSCHAFT UND WERKSTOFFTECHNIK
ISSN0933-5137
Volume51Issue:4Pages:480-487
AbstractIn this investigation, the mixed gamma-GPS/BTSE silane solution for preparing well adhered composite gamma-GPS/BTSE silane film on Q235 carbon steel surface has been successfully optimized by orthogonal test, and the curing process parameters of temperature and time have also been optimized. The results indicate that the optimized hydrolysis parameters for mixed silanes agent solution are as follows: V-ethanol/V-water 3 : 1, V gamma-GPS/V-BTSE 2 : 3, V-silanes 6 vol.%, pH 4.0 and hydrolysis time 72 h. In addition, the optimized curing condition for composite gamma-GPS/BTSE silane film is 120 degrees C and 30 min. After immersion in the optimized mixed gamma-GPS/BTSE silanes agent solution and curing under the optimized condition, the prepared composite gamma-GPS/BTSE silane film on Q235 steel surface can have an adhesion strength of 24.52 MPa to underlying steel substrate.
KeywordEpoxy resin silane treatment orthogonal test adhesion Q235 steel
DOI10.1002/mawe.201900150
Indexed BySCI
Language英语
WOS Research AreaMaterials Science
WOS SubjectMaterials Science, Multidisciplinary
WOS IDWOS:000525608800008
PublisherWILEY-V C H VERLAG GMBH
Citation statistics
Cited Times:1[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.imr.ac.cn/handle/321006/138353
Collection中国科学院金属研究所
Corresponding AuthorSun, Z. D.
Affiliation1.Northeastern Univ, Sch Met, Shenyang 110819, Peoples R China
2.Shenyang Inst Engn, Shenyang 110136, Peoples R China
3.Chinese Acad Sci, Inst Met Res, Lab Corros & Protect Met, Shenyang 110016, Peoples R China
4.Shanghai Univ, Sch Mat Sci & Engn, State Key Lab Adv Special Steel, Shanghai 200072, Peoples R China
Recommended Citation
GB/T 7714
Sun, Z. D.,Yang, Y. N.,Li, Q. K.,et al. Optimization of mixed silanes agent solution and curing process for composite gamma-glycidoxypropyl trimethoxysilane (gamma-GPS)/bis-1.2-(triethoxysilyl)ethane (BTSE) silane film on Q235 steel surfaceOptimierung von vermengten Silanlosungen und Aushartung fur gamma-glycidoxypropyl trimethoxysilan (gamma-GPS)/bis-1,2-(triethoxysilyl)athan (BTSE)-Komposit-Silanschicht auf einer Stahloberflache (Q 235)[J]. MATERIALWISSENSCHAFT UND WERKSTOFFTECHNIK,2020,51(4):480-487.
APA Sun, Z. D.,Yang, Y. N.,Li, Q. K.,Liu, J. G.,Xu, Q.,&Yan, C. W..(2020).Optimization of mixed silanes agent solution and curing process for composite gamma-glycidoxypropyl trimethoxysilane (gamma-GPS)/bis-1.2-(triethoxysilyl)ethane (BTSE) silane film on Q235 steel surfaceOptimierung von vermengten Silanlosungen und Aushartung fur gamma-glycidoxypropyl trimethoxysilan (gamma-GPS)/bis-1,2-(triethoxysilyl)athan (BTSE)-Komposit-Silanschicht auf einer Stahloberflache (Q 235).MATERIALWISSENSCHAFT UND WERKSTOFFTECHNIK,51(4),480-487.
MLA Sun, Z. D.,et al."Optimization of mixed silanes agent solution and curing process for composite gamma-glycidoxypropyl trimethoxysilane (gamma-GPS)/bis-1.2-(triethoxysilyl)ethane (BTSE) silane film on Q235 steel surfaceOptimierung von vermengten Silanlosungen und Aushartung fur gamma-glycidoxypropyl trimethoxysilan (gamma-GPS)/bis-1,2-(triethoxysilyl)athan (BTSE)-Komposit-Silanschicht auf einer Stahloberflache (Q 235)".MATERIALWISSENSCHAFT UND WERKSTOFFTECHNIK 51.4(2020):480-487.
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