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Preparation of highly dispersed antimony-doped tin oxide nano-powder via ion-exchange hydrolysis of SnCl4 and SbCl3 and azeotropic drying
Alternative TitlePreparation of Highly Dispersed Antimony-doped Tin Oxide Nano-powder via Ion-exchange Hydrolysis of SnCl_4 and SbCl_3 and Azeotropic Drying
Yang Fen1; Zhang Xuejun3; Tian Fang1; Wu Xu1; Gan Fuxing1
2007
Source PublicationCHINESE JOURNAL OF AERONAUTICS
ISSN1000-9361
Volume20Issue:2Pages:181-186
AbstractAntimony-doped tin hydroxide colloid precipitates have been synthesized by hydrolysis of SnCl4 and SbCl3 using: (1) an ion-exchange hydrolysis to remove chlorine ions, and (2) isoamyl acetate as an azeotropic solvent to obviate water. The obtained dried powder is of high dispersivity without any need for further grinding. The size and dispersivity of the final particles are investigated with the aid of TG-DTA, BET, XRD and TEM. After having calcined, the antimony-doped tin oxide nanopowder possesses a tetragonal rutile structure with high dispersivity, uniform particles and low hard agglomeration.
Other AbstractAntimony-doped tin hydroxide colloid precipitates have been synthesized by hydrolysis of SnCl4 and SbCl3 using: (1) an ion-exchange hydrolysis to remove chlorine ions, and (2) isoamyl acetate as an azeotropic solvent to obviate water. The obtained dried powder is of high dispersivity without any need for further grinding. The size and dispersivity of the final particles are investigated with the aid of TG-DTA, BET, XRD and TEM. After having calcined, the antimony-doped tin oxide nanopowder possesses a tetragonal rutile structure with high dispersivity, uniform particles and low hard agglomeration.
Keywordantimony-doped tin oxide ion-exchange iso-amyl acetate dispersivity
Indexed ByCSCD
Language英语
CSCD IDCSCD:2911963
Citation statistics
Document Type期刊论文
Identifierhttp://ir.imr.ac.cn/handle/321006/144195
Collection中国科学院金属研究所
Affiliation1.武汉大学
2.曲靖师范学院
3.贵州大学
4.中国科学院金属研究所
Recommended Citation
GB/T 7714
Yang Fen,Zhang Xuejun,Tian Fang,et al. Preparation of highly dispersed antimony-doped tin oxide nano-powder via ion-exchange hydrolysis of SnCl4 and SbCl3 and azeotropic drying[J]. CHINESE JOURNAL OF AERONAUTICS,2007,20(2):181-186.
APA Yang Fen,Zhang Xuejun,Tian Fang,Wu Xu,&Gan Fuxing.(2007).Preparation of highly dispersed antimony-doped tin oxide nano-powder via ion-exchange hydrolysis of SnCl4 and SbCl3 and azeotropic drying.CHINESE JOURNAL OF AERONAUTICS,20(2),181-186.
MLA Yang Fen,et al."Preparation of highly dispersed antimony-doped tin oxide nano-powder via ion-exchange hydrolysis of SnCl4 and SbCl3 and azeotropic drying".CHINESE JOURNAL OF AERONAUTICS 20.2(2007):181-186.
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