Preparation of highly dispersed antimony-doped tin oxide nano-powder via ion-exchange hydrolysis of SnCl4 and SbCl3 and azeotropic drying

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	Preparation of highly dispersed antimony-doped tin oxide nano-powder via ion-exchange hydrolysis of SnCl4 and SbCl3 and azeotropic drying
其他题名	Preparation of Highly Dispersed Antimony-doped Tin Oxide Nano-powder via Ion-exchange Hydrolysis of SnCl_4 and SbCl_3 and Azeotropic Drying
	Yang Fen 1; Zhang Xuejun 3; Tian Fang 1; Wu Xu 1; Gan Fuxing 1
	2007
发表期刊	CHINESE JOURNAL OF AERONAUTICS
ISSN	1000-9361
卷号	20 期号:2 页码:181-186
摘要	Antimony-doped tin hydroxide colloid precipitates have been synthesized by hydrolysis of SnCl4 and SbCl3 using: (1) an ion-exchange hydrolysis to remove chlorine ions, and (2) isoamyl acetate as an azeotropic solvent to obviate water. The obtained dried powder is of high dispersivity without any need for further grinding. The size and dispersivity of the final particles are investigated with the aid of TG-DTA, BET, XRD and TEM. After having calcined, the antimony-doped tin oxide nanopowder possesses a tetragonal rutile structure with high dispersivity, uniform particles and low hard agglomeration.
其他摘要	Antimony-doped tin hydroxide colloid precipitates have been synthesized by hydrolysis of SnCl4 and SbCl3 using: (1) an ion-exchange hydrolysis to remove chlorine ions, and (2) isoamyl acetate as an azeotropic solvent to obviate water. The obtained dried powder is of high dispersivity without any need for further grinding. The size and dispersivity of the final particles are investigated with the aid of TG-DTA, BET, XRD and TEM. After having calcined, the antimony-doped tin oxide nanopowder possesses a tetragonal rutile structure with high dispersivity, uniform particles and low hard agglomeration.
关键词	antimony-doped tin oxide ion-exchange iso-amyl acetate dispersivity
收录类别	CSCD
语种	英语
CSCD记录号	CSCD:2911963
引用统计	被引频次：2[CSCD] [CSCD记录]
文献类型	期刊论文
条目标识符	http://ir.imr.ac.cn/handle/321006/144195
专题	中国科学院金属研究所
作者单位	1.武汉大学 2.曲靖师范学院 3.贵州大学 4.中国科学院金属研究所
推荐引用方式 GB/T 7714	Yang Fen,Zhang Xuejun,Tian Fang,et al. Preparation of highly dispersed antimony-doped tin oxide nano-powder via ion-exchange hydrolysis of SnCl4 and SbCl3 and azeotropic drying[J]. CHINESE JOURNAL OF AERONAUTICS,2007,20(2):181-186.
APA	Yang Fen,Zhang Xuejun,Tian Fang,Wu Xu,&Gan Fuxing.(2007).Preparation of highly dispersed antimony-doped tin oxide nano-powder via ion-exchange hydrolysis of SnCl4 and SbCl3 and azeotropic drying.CHINESE JOURNAL OF AERONAUTICS,20(2),181-186.
MLA	Yang Fen,et al."Preparation of highly dispersed antimony-doped tin oxide nano-powder via ion-exchange hydrolysis of SnCl4 and SbCl3 and azeotropic drying".CHINESE JOURNAL OF AERONAUTICS 20.2(2007):181-186.