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Screening and identification of multi-classified components in Liushenwan using multi-dimension high performance liquid chromatography tandem mass spectrometry system
Alternative TitleScreening and Identification of Multi-classified Components in Liushenwan Using Multi-dimension High Performance Liquid Chromatography Tandem Mass Spectrometry System
Cao Yang1; Liang QiongLin2; Zhang HongYang2; Wang YiMing2; Bi KaiShun1; Luo GuoAn2
2008
Source PublicationCHINESE JOURNAL OF ANALYTICAL CHEMISTRY
ISSN0253-3820
Volume36Issue:1Pages:39-46
AbstractA multi-dimension HPLC/MS(MSn) analytical model using a combination of HPLC/TOF-MS and HPLC/Ion Trap MS' was used to systemically screen and identify multi-classified components in a traditional Chinese medicine formula Liushenwan. Benefit from combining the accurate mass measurement of HPLC/TOF-MS to generate elemental compositions and the complementary multilevel structural information provided by HPLC/Ion Trap MS', 25 components in Liushenwan were identified in all, the corresponding standards were used for corroboration. All the components identified were surveyed and classified according to their medicinal materials derivation (Musk (Moschus berezovskii Flerov), bezoar (Bos Taurus domesticus Gmelin) and toad venom ( Bufo gargarizans Cantor)). This study is expected to provide an effective and reliable pattern for comprehensive and systematic characterization of the complex systems.
KeywordTRADITIONAL CHINESE MEDICINE BUFADIENOLIDES LC/MS/MS PLANT multi-dimension high performance liquid chromatography tandem mass spectrometry Liushenwan systemic screening and identification high performance liquid chromatography-time of flight mass spectrometry
Indexed ByCSCD
Language英语
CSCD IDCSCD:3263981
Citation statistics
Cited Times:7[CSCD]   [CSCD Record]
Document Type期刊论文
Identifierhttp://ir.imr.ac.cn/handle/321006/150448
Collection中国科学院金属研究所
Affiliation1.中国科学院金属研究所
2.清华大学
Recommended Citation
GB/T 7714
Cao Yang,Liang QiongLin,Zhang HongYang,et al. Screening and identification of multi-classified components in Liushenwan using multi-dimension high performance liquid chromatography tandem mass spectrometry system[J]. CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,2008,36(1):39-46.
APA Cao Yang,Liang QiongLin,Zhang HongYang,Wang YiMing,Bi KaiShun,&Luo GuoAn.(2008).Screening and identification of multi-classified components in Liushenwan using multi-dimension high performance liquid chromatography tandem mass spectrometry system.CHINESE JOURNAL OF ANALYTICAL CHEMISTRY,36(1),39-46.
MLA Cao Yang,et al."Screening and identification of multi-classified components in Liushenwan using multi-dimension high performance liquid chromatography tandem mass spectrometry system".CHINESE JOURNAL OF ANALYTICAL CHEMISTRY 36.1(2008):39-46.
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