| Effect of Heat Treatment Method on Microstructure of Tailings Glass Ceramics | |
| Alternative Title | Effect of Heat Treatment Method on Microstructure of Tailings Glass Ceramics |
| Liu Jun; Ou Yang; Xu Changwei; Qi Hong | |
| 2008 | |
| Source Publication | JOURNAL OF WUHAN UNIVERSITY OF TECHNOLOGY-MATERIALS SCIENCE EDITION
 |
| ISSN | 1000-2413 |
| Volume | 23Issue:6Pages:883-888 |
| Abstract | A Cao-Mgo-Al(2)O(3)-SiO(2) quaternary system was established with the main crystal phase design based on Diopside, and the effect of once-through sintering heat treatment on microstructure of iron tailings glass ceramics was studied by using DTA, SEM along with measurement of microhardness and volume density. The experimental results show that, when the total amount of FeO and Fe(2)O(3) exceeds 10wt%, a large number of fine nuclei are produced in the annealing process, and the phenomenon of nucleus resorption happens during the process of nucleation heat treatment, which is unfavorable for preparing iron tailings glass ceramics through once-through sintering method. When the annealing temperature from 1250 degrees C to 830 degrees C, setting crystallization time for 4h, without heat treatment, crystals are well grown with arrangement and interlocking in glass phase. At 830 degrees C the crystals are well developed, well distributed and of good size; with crystallization time of 4 h the crystals with radial shape have high content and regular arrangement. |
| Other Abstract | A Cao-Mgo-Al_2O_3-SiO_2 quaternary system was established with the main crystal phase design based on Diopside, and the effect of once-through sintering heat treatment on microstructure of iron tailings glass ceramics was studied by using DTA, SEM along with measurement of microhardness and volume density. The experimental results show that, when the total amount of FeO and Fe_2O_3 exceeds 10wt%, a large number of fine nuclei are produced in the annealing process, and the phenomenon of nucleus resorption happens during the process of nucleation heat treatment, which is unfavorable for preparing iron tailings glass ceramics through once-through sintering method. When the annealing temperature from 1250 ℃ to 830 ℃, setting crystallization time for 4h, without heat treatment, crystals are well grown with arrangement and interlocking in glass phase. At 830 ℃ the crystals are well developed, well distributed and of good size; with crystallization time of 4 h the crystals with radial shape have high content and regular arrangement. |
| Keyword | one-time sintering heat treatment glass ceramics microstructure |
| Indexed By | CSCD |
| Language | 英语 |
| Funding Project | [State Administration of Foreign Experts Affairs] ; [Younger Natural Science Foundation of Liaoning] |
| CSCD ID | CSCD:3585638 |
| Citation statistics | |
| Document Type | 期刊论文 |
| Identifier | http://ir.imr.ac.cn/handle/321006/154547 |
| Collection | 中国科学院金属研究所 |
| Affiliation | 中国科学院金属研究所 |
| Recommended Citation GB/T 7714 | Liu Jun,Ou Yang,Xu Changwei,et al. Effect of Heat Treatment Method on Microstructure of Tailings Glass Ceramics[J]. JOURNAL OF WUHAN UNIVERSITY OF TECHNOLOGY-MATERIALS SCIENCE EDITION,2008,23(6):883-888. |
| APA | Liu Jun,Ou Yang,Xu Changwei,&Qi Hong.(2008).Effect of Heat Treatment Method on Microstructure of Tailings Glass Ceramics.JOURNAL OF WUHAN UNIVERSITY OF TECHNOLOGY-MATERIALS SCIENCE EDITION,23(6),883-888. |
| MLA | Liu Jun,et al."Effect of Heat Treatment Method on Microstructure of Tailings Glass Ceramics".JOURNAL OF WUHAN UNIVERSITY OF TECHNOLOGY-MATERIALS SCIENCE EDITION 23.6(2008):883-888. |
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