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Technical Note: A High-Temperature, High-Pressure Window for In Situ Optical Observation and Raman Detection
Kuang, Wenjun; Wu, Xinqiang; Wang, Xiang; Han, En-Hou; xqwu@imr.ac.cn
2015
Source PublicationCORROSION
ISSN0010-9312
Volume71Issue:6Pages:687-691
AbstractA window was developed on a high-temperature, high-pressure refreshed autoclave to perform in situ tests. High-purity single crystal sapphire was used as window material to withstand the harsh environment and minimize the production of fluorescence. The cone-shaped internal structure enables a large light flux necessary for the in situ optical observation. Through this window, in situ optical observation and Raman tests were successfully performed in high-temperature, high-pressure water using a long-distance microscope and a custom-made Raman system. The formation of spinel oxide on 304 stainless steel in oxygenated water containing a high concentration of Ni cations was verified by in situ Raman tests.
description.department[kuang, wenjun ; wu, xinqiang ; wang, xiang ; han, en-hou] chinese acad sci, inst met res, key lab nucl mat & safety assessment, liaoning key lab safety & assessment tech nucl ma, shenyang 110016, peoples r china ; [kuang, wenjun] univ michigan, ann arbor, mi 48109 usa ; [kuang, wenjun] chinese acad sci, inst met res, shenyang 110016, peoples r china
KeywordCracking Oxidation Raman Spectroscopy
Funding OrganizationScience and Technology Foundation of China [51371174]; Special Funds for the Major State Basic Research Projects [2011CB610505]; Innovation Fund of Institute of Metal Research, Chinese Academy of Sciences
Indexed Bysci
Language英语
WOS IDWOS:000355559700001
Citation statistics
Cited Times:2[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.imr.ac.cn/handle/321006/75178
Collection中国科学院金属研究所
Corresponding Authorxqwu@imr.ac.cn
Recommended Citation
GB/T 7714
Kuang, Wenjun,Wu, Xinqiang,Wang, Xiang,et al. Technical Note: A High-Temperature, High-Pressure Window for In Situ Optical Observation and Raman Detection[J]. CORROSION,2015,71(6):687-691.
APA Kuang, Wenjun,Wu, Xinqiang,Wang, Xiang,Han, En-Hou,&xqwu@imr.ac.cn.(2015).Technical Note: A High-Temperature, High-Pressure Window for In Situ Optical Observation and Raman Detection.CORROSION,71(6),687-691.
MLA Kuang, Wenjun,et al."Technical Note: A High-Temperature, High-Pressure Window for In Situ Optical Observation and Raman Detection".CORROSION 71.6(2015):687-691.
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