Technical Note: A High-Temperature, High-Pressure Window for In Situ Optical Observation and Raman Detection

IMR OpenIR

	Technical Note: A High-Temperature, High-Pressure Window for In Situ Optical Observation and Raman Detection
	Kuang, Wenjun; Wu, Xinqiang; Wang, Xiang; Han, En-Hou; xqwu@imr.ac.cn
	2015
发表期刊	CORROSION
ISSN	0010-9312
卷号	71 期号:6 页码:687-691
摘要	A window was developed on a high-temperature, high-pressure refreshed autoclave to perform in situ tests. High-purity single crystal sapphire was used as window material to withstand the harsh environment and minimize the production of fluorescence. The cone-shaped internal structure enables a large light flux necessary for the in situ optical observation. Through this window, in situ optical observation and Raman tests were successfully performed in high-temperature, high-pressure water using a long-distance microscope and a custom-made Raman system. The formation of spinel oxide on 304 stainless steel in oxygenated water containing a high concentration of Ni cations was verified by in situ Raman tests.
部门归属	[kuang, wenjun ; wu, xinqiang ; wang, xiang ; han, en-hou] chinese acad sci, inst met res, key lab nucl mat & safety assessment, liaoning key lab safety & assessment tech nucl ma, shenyang 110016, peoples r china ; [kuang, wenjun] univ michigan, ann arbor, mi 48109 usa ; [kuang, wenjun] chinese acad sci, inst met res, shenyang 110016, peoples r china
关键词	Cracking Oxidation Raman Spectroscopy
资助者	Science and Technology Foundation of China [51371174]; Special Funds for the Major State Basic Research Projects [2011CB610505]; Innovation Fund of Institute of Metal Research, Chinese Academy of Sciences
收录类别	sci
语种	英语
文献类型	期刊论文
条目标识符	http://ir.imr.ac.cn/handle/321006/75178
专题	中国科学院金属研究所
通讯作者	xqwu@imr.ac.cn
推荐引用方式 GB/T 7714	Kuang, Wenjun,Wu, Xinqiang,Wang, Xiang,et al. Technical Note: A High-Temperature, High-Pressure Window for In Situ Optical Observation and Raman Detection[J]. CORROSION,2015,71(6):687-691.
APA	Kuang, Wenjun,Wu, Xinqiang,Wang, Xiang,Han, En-Hou,&xqwu@imr.ac.cn.(2015).Technical Note: A High-Temperature, High-Pressure Window for In Situ Optical Observation and Raman Detection.CORROSION,71(6),687-691.
MLA	Kuang, Wenjun,et al."Technical Note: A High-Temperature, High-Pressure Window for In Situ Optical Observation and Raman Detection".CORROSION 71.6(2015):687-691.