| Synthesis and TEM observation of fluffy hollow carbon spheres by FeCl3 catalyzed solvent-thermal reaction | |
| Yin, Cailiu; Huang, Qizhong; Liu, Baorong; Wang, Xiufei; Xie, Yonggui; He, Lianlong; Zhang, Mingyu; Yang, Xin | |
| Corresponding Author | Huang, Qizhong(qzhuang@mail.csu.edu.cn) |
| 2007-08-01 | |
| Source Publication | MATERIALS LETTERS
 |
| ISSN | 0167-577X |
| Volume | 61Issue:19-20Pages:4015-4018 |
| Abstract | Fluffy hollow carbon spheres with the diameter of 0.3-1.8 mu m and shell thickness of 30-80 nm were successfully synthesized via FeCl3 catalyzed solvent-thermal reaction in a scaled autoclave at 350 degrees C for 3 h, with CaC2 and CCl4 as carbon sources and reactants. XRD and TEM observations verify that the fluffy hollow carbon spheres are composed of curved and disordered carbon flakes with the interlayer instance of approximate 0.35 nm. Furthermore, MCNTs with Fe-Mn-Cr nanorods encapsulated are also observed. A possible growth mechanism for the fluffy hollow carbon sphere is proposed. (c) 2007 Elsevier B.V. All rights reserved. |
| Keyword | hollow carbon spheres solvent-thermal reaction electron microscopy microstructure |
| DOI | 10.1016/j.matlet.2007.01.008 |
| Indexed By | SCI |
| Language | 英语 |
| WOS Research Area | Materials Science ; Physics |
| WOS Subject | Materials Science, Multidisciplinary ; Physics, Applied |
| WOS ID | WOS:000248155900001 |
| Publisher | ELSEVIER SCIENCE BV |
| Citation statistics | |
| Document Type | 期刊论文 |
| Identifier | http://ir.imr.ac.cn/handle/321006/91197 |
| Collection | 中国科学院金属研究所 |
| Corresponding Author | Huang, Qizhong |
| Affiliation | 1.Cent S Univ, State Key Lab Powder Met, Changsha 410083, Peoples R China 2.Guangxi Univ, Coll Phys Sci & Engn, Nanning 530004, Peoples R China 3.Chinese Acad Sci, Inst Met Res, Shenyang Natl Lab Mat Sci, Shenyang 110016, Peoples R China |
| Recommended Citation GB/T 7714 | Yin, Cailiu,Huang, Qizhong,Liu, Baorong,et al. Synthesis and TEM observation of fluffy hollow carbon spheres by FeCl3 catalyzed solvent-thermal reaction[J]. MATERIALS LETTERS,2007,61(19-20):4015-4018. |
| APA | Yin, Cailiu.,Huang, Qizhong.,Liu, Baorong.,Wang, Xiufei.,Xie, Yonggui.,...&Yang, Xin.(2007).Synthesis and TEM observation of fluffy hollow carbon spheres by FeCl3 catalyzed solvent-thermal reaction.MATERIALS LETTERS,61(19-20),4015-4018. |
| MLA | Yin, Cailiu,et al."Synthesis and TEM observation of fluffy hollow carbon spheres by FeCl3 catalyzed solvent-thermal reaction".MATERIALS LETTERS 61.19-20(2007):4015-4018. |
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