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Synthesis and TEM observation of fluffy hollow carbon spheres by FeCl3 catalyzed solvent-thermal reaction
Yin, Cailiu; Huang, Qizhong; Liu, Baorong; Wang, Xiufei; Xie, Yonggui; He, Lianlong; Zhang, Mingyu; Yang, Xin
Corresponding AuthorHuang, Qizhong(qzhuang@mail.csu.edu.cn)
2007-08-01
Source PublicationMATERIALS LETTERS
ISSN0167-577X
Volume61Issue:19-20Pages:4015-4018
AbstractFluffy hollow carbon spheres with the diameter of 0.3-1.8 mu m and shell thickness of 30-80 nm were successfully synthesized via FeCl3 catalyzed solvent-thermal reaction in a scaled autoclave at 350 degrees C for 3 h, with CaC2 and CCl4 as carbon sources and reactants. XRD and TEM observations verify that the fluffy hollow carbon spheres are composed of curved and disordered carbon flakes with the interlayer instance of approximate 0.35 nm. Furthermore, MCNTs with Fe-Mn-Cr nanorods encapsulated are also observed. A possible growth mechanism for the fluffy hollow carbon sphere is proposed. (c) 2007 Elsevier B.V. All rights reserved.
Keywordhollow carbon spheres solvent-thermal reaction electron microscopy microstructure
DOI10.1016/j.matlet.2007.01.008
Indexed BySCI
Language英语
WOS Research AreaMaterials Science ; Physics
WOS SubjectMaterials Science, Multidisciplinary ; Physics, Applied
WOS IDWOS:000248155900001
PublisherELSEVIER SCIENCE BV
Citation statistics
Cited Times:15[WOS]   [WOS Record]     [Related Records in WOS]
Document Type期刊论文
Identifierhttp://ir.imr.ac.cn/handle/321006/91197
Collection中国科学院金属研究所
Corresponding AuthorHuang, Qizhong
Affiliation1.Cent S Univ, State Key Lab Powder Met, Changsha 410083, Peoples R China
2.Guangxi Univ, Coll Phys Sci & Engn, Nanning 530004, Peoples R China
3.Chinese Acad Sci, Inst Met Res, Shenyang Natl Lab Mat Sci, Shenyang 110016, Peoples R China
Recommended Citation
GB/T 7714
Yin, Cailiu,Huang, Qizhong,Liu, Baorong,et al. Synthesis and TEM observation of fluffy hollow carbon spheres by FeCl3 catalyzed solvent-thermal reaction[J]. MATERIALS LETTERS,2007,61(19-20):4015-4018.
APA Yin, Cailiu.,Huang, Qizhong.,Liu, Baorong.,Wang, Xiufei.,Xie, Yonggui.,...&Yang, Xin.(2007).Synthesis and TEM observation of fluffy hollow carbon spheres by FeCl3 catalyzed solvent-thermal reaction.MATERIALS LETTERS,61(19-20),4015-4018.
MLA Yin, Cailiu,et al."Synthesis and TEM observation of fluffy hollow carbon spheres by FeCl3 catalyzed solvent-thermal reaction".MATERIALS LETTERS 61.19-20(2007):4015-4018.
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