Synthesis and TEM observation of fluffy hollow carbon spheres by FeCl3 catalyzed solvent-thermal reaction

doi:10.1016/j.matlet.2007.01.008

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	Synthesis and TEM observation of fluffy hollow carbon spheres by FeCl3 catalyzed solvent-thermal reaction
	Yin, Cailiu ; Huang, Qizhong ; Liu, Baorong ; Wang, Xiufei ; Xie, Yonggui ; He, Lianlong ; Zhang, Mingyu ; Yang, Xin
通讯作者	Huang, Qizhong(qzhuang@mail.csu.edu.cn)
	2007-08-01
发表期刊	MATERIALS LETTERS
ISSN	0167-577X
卷号	61 期号:19-20 页码:4015-4018
摘要	Fluffy hollow carbon spheres with the diameter of 0.3-1.8 mu m and shell thickness of 30-80 nm were successfully synthesized via FeCl3 catalyzed solvent-thermal reaction in a scaled autoclave at 350 degrees C for 3 h, with CaC2 and CCl4 as carbon sources and reactants. XRD and TEM observations verify that the fluffy hollow carbon spheres are composed of curved and disordered carbon flakes with the interlayer instance of approximate 0.35 nm. Furthermore, MCNTs with Fe-Mn-Cr nanorods encapsulated are also observed. A possible growth mechanism for the fluffy hollow carbon sphere is proposed. (c) 2007 Elsevier B.V. All rights reserved.
关键词	hollow carbon spheres solvent-thermal reaction electron microscopy microstructure
DOI	10.1016/j.matlet.2007.01.008
收录类别	SCI
语种	英语
WOS研究方向	Materials Science ; Physics
WOS类目	Materials Science, Multidisciplinary ; Physics, Applied
WOS记录号	WOS:000248155900001
出版者	ELSEVIER SCIENCE BV
引用统计	被引频次：18[WOS] [WOS记录] [WOS相关记录]
文献类型	期刊论文
条目标识符	http://ir.imr.ac.cn/handle/321006/91197
专题	中国科学院金属研究所
通讯作者	Huang, Qizhong
作者单位	1.Cent S Univ, State Key Lab Powder Met, Changsha 410083, Peoples R China 2.Guangxi Univ, Coll Phys Sci & Engn, Nanning 530004, Peoples R China 3.Chinese Acad Sci, Inst Met Res, Shenyang Natl Lab Mat Sci, Shenyang 110016, Peoples R China
推荐引用方式 GB/T 7714	Yin, Cailiu,Huang, Qizhong,Liu, Baorong,et al. Synthesis and TEM observation of fluffy hollow carbon spheres by FeCl3 catalyzed solvent-thermal reaction[J]. MATERIALS LETTERS,2007,61(19-20):4015-4018.
APA	Yin, Cailiu.,Huang, Qizhong.,Liu, Baorong.,Wang, Xiufei.,Xie, Yonggui.,...&Yang, Xin.(2007).Synthesis and TEM observation of fluffy hollow carbon spheres by FeCl3 catalyzed solvent-thermal reaction.MATERIALS LETTERS,61(19-20),4015-4018.
MLA	Yin, Cailiu,et al."Synthesis and TEM observation of fluffy hollow carbon spheres by FeCl3 catalyzed solvent-thermal reaction".MATERIALS LETTERS 61.19-20(2007):4015-4018.