Synthesis of Ti3SiC2 by high energy ball milling and reactive sintering from Ti, Si, and C elements

doi:10.1016/j.jnucmat.2008.12.321

IMR OpenIR

	Synthesis of Ti3SiC2 by high energy ball milling and reactive sintering from Ti, Si, and C elements
	Meng, Fanling 1,2,3; Chaffron, Laurent 1; Zhou, Yanchun 3
通讯作者	Chaffron, Laurent(laurent.chaffron@cea.fr)
	2009-04-30
发表期刊	JOURNAL OF NUCLEAR MATERIALS
ISSN	0022-3115
卷号	386-88 页码:647-649
摘要	We present an original method of preparation of nanostructured Ti3SiC2 compound based on high energy ball milling and reactive sintering techniques. Starting materials are Ti, Si, and C elements. X-ray diffraction and secondary electron microscopy are used to identify the formed phases and to analyze the obtained microstructures. Lower milling intensity and shorter milling time are found as the best milling conditions in order to get an intimate mixture of the three elements without formation of detectable secondary phases. The optimized sintering temperature is equal to 1350 degrees C. A method used for minimizing the oxygen content in the final compound is presented. (c) 2008 Elsevier B.V. All rights reserved.
DOI	10.1016/j.jnucmat.2008.12.321
收录类别	SCI
语种	英语
WOS研究方向	Materials Science ; Nuclear Science & Technology ; Mining & Mineral Processing
WOS类目	Materials Science, Multidisciplinary ; Nuclear Science & Technology ; Mining & Mineral Processing
WOS记录号	WOS:000266386900161
出版者	ELSEVIER SCIENCE BV
引用统计	被引频次：16[WOS] [WOS记录] [WOS相关记录]
文献类型	期刊论文
条目标识符	http://ir.imr.ac.cn/handle/321006/99108
专题	中国科学院金属研究所
通讯作者	Chaffron, Laurent
作者单位	1.CEA Saclay, DENDANS, DMN, SRMP,SRMA,LTMEX, F-91191 Gif Sur Yvette, France 2.Chinese Acad Sci, Grad Sch, Inst Met Res, Shenyang Natl Lab Mat Sci, Beijing 100039, Peoples R China 3.Chinese Acad Sci, Inst Met Res, Shenyang Natl Lab Mat Sci, Shenyang 110016, Peoples R China
推荐引用方式 GB/T 7714	Meng, Fanling,Chaffron, Laurent,Zhou, Yanchun. Synthesis of Ti3SiC2 by high energy ball milling and reactive sintering from Ti, Si, and C elements[J]. JOURNAL OF NUCLEAR MATERIALS,2009,386-88:647-649.
APA	Meng, Fanling,Chaffron, Laurent,&Zhou, Yanchun.(2009).Synthesis of Ti3SiC2 by high energy ball milling and reactive sintering from Ti, Si, and C elements.JOURNAL OF NUCLEAR MATERIALS,386-88,647-649.
MLA	Meng, Fanling,et al."Synthesis of Ti3SiC2 by high energy ball milling and reactive sintering from Ti, Si, and C elements".JOURNAL OF NUCLEAR MATERIALS 386-88(2009):647-649.